Distillation equipment capable of controlling temperature of condenser pipe and viscosity of fraction in real time and control method of distillation equipment

A technology for real-time control and distillation equipment, applied in the direction of distillation adjustment/control, boiler/distillate distillation, etc.

Active Publication Date: 2021-05-07
SHAANXI YANCHANG PETROLEUM GRP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In order to solve the defects in the prior art, the object of the present invention is to provide a distillation equipment and its control method for real-time control of the temperature of the condensation pipe and the viscosity of the distillate, which can control the temperature of the condensation pipe and the temperature of the collector through real-time pressure display. The viscosity of the distillate can prevent the blockage of the condensation pipe and the collector, and has the advantages of reasonable structure, simple operation, real-time automatic control, practical and efficient

Method used

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  • Distillation equipment capable of controlling temperature of condenser pipe and viscosity of fraction in real time and control method of distillation equipment
  • Distillation equipment capable of controlling temperature of condenser pipe and viscosity of fraction in real time and control method of distillation equipment
  • Distillation equipment capable of controlling temperature of condenser pipe and viscosity of fraction in real time and control method of distillation equipment

Examples

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Embodiment 1

[0032] Embodiment 1: The distillation sample is medium and low temperature coal tar from a certain factory;

[0033] A method for controlling the temperature of the condenser tube and the viscosity of the distillate, specifically comprising the steps of:

[0034] Step 1. According to the formula: Input the control variables k=1.5, b=10, c=15 in the circulating water bath control unit 8, and input the initial temperature of 20°C and the maximum limit temperature of 200°C, collect the measured viscosity value v of the viscosity sensor in the distillation process in real time, and calculate The theoretical circulation temperature T of the cold bath;

[0035] Step 2: 20°C is used as the starting temperature of the circulation temperature of the cold bath, and the circulating water bath control unit 8 compares in real time the current actually measured circulation temperature of the cold bath with the theoretical circulation temperature T of the cold bath obtained according to th...

Embodiment 2

[0038] Embodiment 2: the distillation sample is dehydrated crude oil of a certain plant;

[0039] A method for controlling the temperature of the condenser tube and the viscosity of the distillate, specifically comprising the steps of:

[0040] Step 1. According to the formula: Input the control variables k=2, b=15, c=10 in the circulating water bath control unit 8, and input the initial temperature of 20°C and the maximum limit temperature of 200°C, collect the measured viscosity value v of the viscosity sensor in the distillation process in real time, and calculate The theoretical circulation temperature T of the cold bath;

[0041] Step 2: 20°C is used as the starting temperature of the circulation temperature of the cold bath, and the circulating water bath control unit 8 compares in real time the current actually measured circulation temperature of the cold bath with the theoretical circulation temperature T of the cold bath obtained according to the formula of step 1. ...

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Abstract

The invention discloses distillation equipment for controlling the temperature of a condenser pipe and the viscosity of fractions in real time and a control method of the distillation equipment. The equipment comprises a heating device, a distillation device and a condensing device which are connected with one another. According to the present invention, the condensation pipe monitoring jacket is arranged on the outer wall of the condensation pipe, the collector monitoring jacket is arranged on the outer wall of the collector, and the circulating water bath control unit is used to perform online viscosity monitoring on the distillate component so as to make the distillate component have flowability in the set range, and if the online viscosity monitoring result shows that the viscosity is not in the normal distillate range, the condensing device is heated through the circulating water bath control unit, and the viscosity of distilled components is reduced when the temperature rises because the temperature and the viscosity have an inverse relation, so the equipment has the advantages of reasonable structure, simplicity in operation, real-time automatic control, practicability and high efficiency.

Description

technical field [0001] The invention relates to the technical field of distillation equipment, in particular to a distillation equipment and a control method thereof for real-time control of the temperature of a condensing tube and the viscosity of a distillate. Background technique [0002] Distillation is a thermodynamic separation process, which is a combination of two unit operations of evaporation and condensation. Compared with other separation methods, such as extraction, filtration and crystallization, its advantage is that it does not need to use other solvents other than system components. This ensures that no new impurities are introduced. [0003] The distillation equipment in the prior art, such as the boiling point distillation device is a set of kettle-type atmospheric and vacuum distillation equipment, which has a strong fractionation ability. After passing through the boiling point distillation device, crude oil and coal tar can be cut into different narrow ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D3/02B01D3/42
CPCB01D3/02B01D3/42
Inventor 杨猛陈刚康徐伟张生娟杜宁赵静党昱
Owner SHAANXI YANCHANG PETROLEUM GRP
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