High nitrogen vanadium titanium alloy and production method thereof
A technology of high-nitrogen vanadium-titanium alloy and nitrogen-vanadium-titanium alloy, which is applied in the field of high-nitrogen vanadium-titanium alloy and its production, and can solve the problems of easy oxidation of titanium, cracking, and difficult absorption.
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example 1
[0047] Take 73KG of ferrotitanium powder containing 40% of titanium and 27KG of ferrovanadium powder containing 50% of vanadium, mix them with a mixer and put them into a high pressure reactor, add silicon powder ignition powder, vacuumize to -0.09MPa, and introduce nitrogen , the pressure is adjusted to 4-12MPa, 3.4 is energized and ignited, and the pressure is maintained. Observe that the reaction temperature drops from the highest point to below 100°C. A high-nitrogen vanadium-titanium alloy is obtained, and the composition is: Ti: 24.2%, V: 11.7%, N: 10.1%.
example 2
[0049] Take 65KG of ferrotitanium powder containing 40% of titanium and 35 kg of ferrovanadium nitride powder containing 43% of vanadium and mix them into a high pressure reactor, add silicon powder ignition powder, evacuate to -0.09MPa, introduce nitrogen, and adjust the pressure. To 4-12MPa, power on and ignite at 3.4, and maintain the pressure. Observe that the reaction temperature drops from the highest point to below 100°C. A high-nitrogen vanadium-titanium alloy is obtained, and the composition is: Ti: 22.4%, V: 12.7%, N: 12.3%.
example 3
[0051] Take 73KG ferrotitanium powder containing 40% titanium and 27KG ferrovanadium powder containing 50% vanadium, mix them with a mixer, press the mixed materials into balls, put them in a drying box and dry them at 110-160℃ for 4- 10 hours. After drying, put it into a kiln, vacuumize it to -0.01MPa, pass in nitrogen-containing gas, adjust the pressure to 0.01-0.04MPa, heat it up to 300-350 ℃ for 4 hours, continue to heat up to 550-650 ℃ for 2 hours, Then cool to room temperature. A high-nitrogen vanadium-titanium alloy is obtained, and the composition is: Ti: 27.4%, V: 13.1%, N: 14.3%.
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