Carbon fiber modification method and product thereof

A carbon fiber modification technology, which is applied in the field of carbon fiber modification methods and its products, can solve the problems of carbon fiber mechanical properties, poor toughness, etc.

Active Publication Date: 2021-07-09
ANHUI UNIVERSITY OF TECHNOLOGY AND SCIENCE +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0002] Carbon fiber is a fiber structure of inorganic carbon materials. It is a microcrystalline graphite material obtained by carbonization and graphitization of inorganic carbon materials. Carbonization and graphitization in the manufacturing process of carbon fibers endow carbon fibers with many excellent properties. High strength and high modulus, good electrical and thermal conductivity, good electromagnetic shielding

Method used

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  • Carbon fiber modification method and product thereof
  • Carbon fiber modification method and product thereof
  • Carbon fiber modification method and product thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0029] (1) Place the bundled 12K carbon fiber produced by Toray in Japan in an acetone solution at a constant temperature of 70°C for 24 hours, then wash it alternately with absolute ethanol and deionized water to remove the sizing agent, dust and oil on the surface of the fiber, and then Dry and cool at 80°C for 24 hours;

[0030] (2) Use the carbon fiber treated in step (1) as the substrate, fix it on the cardboard in parallel, install the carbon target on the cathode plate, place the substrate under the substrate support, and perform magnetron sputtering under the following conditions Processing: sputtering power 250W, magnetron sputtering pressure 1Pa, sputtering time 30min, background vacuum 2×10 -3 Pa, the distance between the target and the substrate is 4 cm, high-purity argon (99.999%) is used as the working gas, the flow rate of the argon gas is 80 ml / min, and the substrate holder rotates at a speed of 30 r / min.

[0031] (3) The carbon fibers treated in step (2) are ...

Embodiment 2

[0039] Same as Example 1, the difference is that the sputtering power is 250W, the magnetron sputtering pressure is 1Pa, the sputtering time is 45min, and finally it is treated in a vacuum furnace at 200°C for 40min. The tensile breaking strength of the treated bundled carbon fiber is 0.8956KN.

Embodiment 3

[0041] Same as Example 1, the difference is that under the condition of 250W, the magnetron sputtering pressure is 1Pa, the sputtering time is 45min, and the heat treatment condition is 300°C for 40min. The tensile breaking strength of the treated bundled carbon fiber is 0.8533KN.

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Abstract

The invention relates to the technical field of modified carbon fibers, in particular to a carbon fiber modification method and a product thereof. Magnetron sputtering treatment is carried out on carbon fibers, and then heating treatment is performed in an inert atmosphere to obtain modified carbon fibers; in the magnetron sputtering treatment, carbon fibers are used as a base material, carbon is used as a target material, and sputtering conditions are as follows: the vacuum degree is 2*10<-3>Pa, the target-substrate distance is 4cm, the magnetron sputtering power is 150-350W, the magnetron sputtering pressure intensity is 0.5-1.6 Pa, the magnetron sputtering time is 20-60min, high-purity argon is used as working gas, and the argon flow is 80ml/min; and the heating treatment conditions are as follows: the heating rate is 5 DEG C/min, the heat treatment temperature is 200-600 DEG C, and the heat treatment time is 25-40 min. According to the carbon fibers modified by the method, the tensile breaking strength can be increased by 4-12%, the tensile breaking work can be increased by 15-40%, and the mechanical property of the carbon fibers can be effectively improved.

Description

technical field [0001] The invention relates to the technical field of carbon fiber modification, in particular to a carbon fiber modification method and a product thereof. Background technique [0002] Carbon fiber is a fiber structure of inorganic carbon materials. It is a microcrystalline graphite material obtained by carbonization and graphitization of inorganic carbon materials. Carbonization and graphitization in the manufacturing process of carbon fibers endow carbon fibers with many excellent properties. High strength and high modulus, good electrical and thermal conductivity, good electromagnetic shielding, good fatigue resistance, is a new generation of reinforced fibers; but carbon fiber itself is a brittle material with poor toughness; in addition, some defects will occur on the surface of the fiber during the preparation process. The mechanical properties are affected during use, so carbon fiber is rarely used alone as a structural material, and is often used as...

Claims

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Application Information

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IPC IPC(8): C23C14/35C23C14/06D06M11/74D06M101/40
CPCC23C14/35C23C14/0605D06M11/74D06M2101/40C23C14/021C23C14/541D06M10/006C23C14/024C23C14/5806
Inventor 杨莉徐珍珍倪庆清陈缘
Owner ANHUI UNIVERSITY OF TECHNOLOGY AND SCIENCE
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