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Dihydrochalcones from balanophora harlandii

A technology of dihydrochalcones and red winter snakes, applied in the field of dihydrochalcones from red winter snakes, can solve problems such as frustrating consumers

Pending Publication Date: 2021-08-31
THE COCA COLA CO
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, non-caloric and low-caloric sweeteners differ from natural caloric sugars in ways that frustrate consumers

Method used

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  • Dihydrochalcones from balanophora harlandii

Examples

Experimental program
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Effect test

example 1

[0228] Example 1: Isolation and Characterization of Analogs from Red Winter Snake

[0229] instrument: 1D and 2D NMR data were recorded on a Bruker Avance III 500 or 600HD spectrometer, and 1 H and 13 C NMR chemical shifts referenced to methanol-d 4 (δH 3.31 and δ C 49.0) and DMSO-d 6 (δH 2.50 and δ C39.52) residual solvent peak. High-resolution electrospray ionization mass spectrometry (HRESIMS) was performed with a Sciex Triple TOF 4600 spectrometer in negative ion mode. GC-MS was performed on an Agilent 7890A / 5977A GC / MSD system using an Agilent HP-5MS column (30 m x 0.25 mm x 0.25 μm). Semi-preparative HPLC was performed on an Agilent 1260infinity with UV detector using a Boston Green ODS-AQ column (10 x 250 mm, 5 μm). Preparative HPLC was performed on a Shimadzu LC-20AP system using a YMC Actus Hydrosphere C18 column (30 x 250 mm, 5 μm) or a YMC Triart ODS column (50 x 250 mm, 7 μm). AB-8 resin (Sunresin New Materials Co. Ltd., China), MCI gel CHP-20 (Mitsubish...

example 2

[0269] Example 2: Sweetness enhancement

[0270] Prepare a sample with the following composition:

[0271] Table 1: 2% CC-00474 in PG

[0272] Element quantity CC-00474 2mg Propylene Glycol 98mg

[0273] Table 2: Rebaudioside M at 250 ppm in acidic water

[0274] Element quantity Rebaudioside M 125mg water 499.75g citric acid 125mg

[0275] Table 3: 20 ppm of CC-00474 and 250 ppm of Rebaudioside M in acidic water

[0276] Element quantity 250ppm Rebaudioside M in acidic water (Table 2) 100g CC-00474 in PG (Table 1) 0.1g

[0277] Table 4: Rebaudioside M and PG at 250 ppm in acidic water (control)

[0278] Element quantity 250ppm Rebaudioside M in acidic water (Table 2) 100g PG 98mg

[0279] Prepare CC-00474 in PG in a weighing boat and add it to the Reb M solution with stirring. Rinse the weighing boat with Reb M solution. The solution was stirred u...

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PUM

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Abstract

Methods of isolating dihydrochalcone compounds of Formula (I) from Balanophora harlandii are provided herein. Compositions and consumables comprising at least one sweetener and at least one dihydrochalcone compound described herein are also provided. Methods of enhancing the sweetness of a consumable, methods of making a consumable taste more like a sucrose-sweetened consumable and methods of preparing consumables are also detailed herein.

Description

[0001] Cross References to Related Applications [0002] This application claims priority to US Provisional Application No. 62 / 749,993, filed October 24, 2019, which is incorporated by reference in its entirety. [0003] field of invention [0004] The present teaching relates to methods of isolating dihydrochalcone compounds from red winter snake mushroom (Balanophora harlandii) and the use of said dihydrochalcone compounds in consumer products. [0005] Background of the invention [0006] Naturally caloric sugars such as sucrose, fructose, and glucose are used to impart a pleasing taste to beverages, foods, pharmaceuticals, and oral hygiene / cosmetic products. In particular, sucrose imparts a consumer preferred taste. While sucrose provides a superior sweetness profile, it is disadvantageously caloric. [0007] No-caloric or low-caloric sweeteners have been introduced to meet consumer demand. However, non-caloric and low-caloric sweeteners differ from natural caloric suga...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07H15/203C07H1/08A23L2/56A23L2/58A23L2/60
CPCA23L2/56A23L2/58C07H15/203A23L2/60C07H1/08A23L2/68A23V2002/00B01D15/325B01D15/426C07H15/207
Inventor 王彬佶·马因德拉·普拉卡什
Owner THE COCA COLA CO
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