Oil-based drilling fluid plugging agent and application thereof
A technology of oil-based drilling fluid and plugging agent, which is applied in the direction of reagents, drilling compositions, chemical instruments and methods, etc., can solve the problems of high construction risk, high use requirements, long time consumption, etc., to save operating time, The effect of low risk of use and improved sealing ability
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Embodiment 1
[0048] This embodiment provides an oil-based drilling fluid plugging agent. The preparation process of the oil-based drilling fluid plugging agent is as follows:
[0049] 1. After heating and melting 100 parts of bisphenol A epoxy resin, add 15 parts of 4,4' diaminodiphenylmethane one by one and stir evenly, solidify at 80°C for 6 hours, then hot press molding, keep pressure and cool to room temperature, The temperature-controlled expansion material is obtained by pulverizing and granulating.
[0050] 2. Mix 60 parts of elastic graphite, 10 parts of powdered asphalt, 10 parts of bamboo fiber, 10 parts of the temperature-controlled expansion material obtained in step 1, and 10 parts of nitrile rubber powder to obtain an oil-based drilling fluid plugging agent.
[0051] 3. The oil-based drilling fluid was prepared in the same way as Comparative Example 1, and the oil-based drilling fluid plugging agent was slowly added to the oil-based drilling fluid according to the addition r...
Embodiment 2
[0053] This embodiment provides an oil-based drilling fluid plugging agent. The preparation process of the oil-based drilling fluid plugging agent is as follows:
[0054] 1. After heating and melting 100 parts of bisphenol A epoxy resin, add 8 parts of 4,4' diaminodiphenylmethane and 5 parts of m-phenylenediamine one by one and stir evenly, cure at 80°C for 2 hours, and heat up to 150°C Solidified for 4 hours, then hot-pressed, cooled to room temperature under pressure, pulverized and granulated to obtain a temperature-controlled expansion material.
[0055] 2. Mix 60 parts of calcium carbonate, 10 parts of powdered asphalt, 10 parts of bamboo fiber, 10 parts of the temperature-controlled expansion material obtained in step 1, and 10 parts of nitrile rubber powder to obtain an oil-based drilling fluid plugging agent.
[0056] 3. The oil-based drilling fluid was prepared in the same way as Comparative Example 1, and the oil-based drilling fluid plugging agent was slowly added ...
Embodiment 3
[0058] This embodiment provides an oil-based drilling fluid plugging agent. The preparation process of the oil-based drilling fluid plugging agent is as follows:
[0059] 1. After heating and melting 100 parts of bisphenol A epoxy resin, add 8 parts of m-phenylenediamine one by one and stir evenly, solidify at 100°C for 6 hours, then hot press molding, keep pressure and cool to room temperature, pulverize and granulate to obtain warm controlled expansion material.
[0060] 2. Mix 60 parts of calcium carbonate, 10 parts of powdered asphalt, 10 parts of bamboo fiber, 10 parts of the temperature-controlled expansion material obtained in step 1, and 10 parts of nitrile rubber powder to obtain an oil-based drilling fluid plugging agent.
[0061] 3. The oil-based drilling fluid was prepared in the same way as Comparative Example 1, and the oil-based drilling fluid plugging agent was slowly added to the oil-based drilling fluid according to the addition ratio of 50g / L, and stirred e...
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