Cu/cu2o interface nanostructures for electrochemical co2 reduction
An electrochemical, CO2 technology, applied in nanotechnology, chemical/physical process, nanotechnology, etc. for materials and surface science, can solve the problems of lack of Cu thin film surface area and active site research
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[0046] Example 1: Using some Cu from Comparative Example 1 2 O crystals to form Cu / Cu according to the present invention 2 O particles. Specifically, 132 mg of Cu of Comparative Example 1 was mixed at room temperature 2 O crystals were added to 40 ml of double distilled HO 2 O and stirred for 10 minutes. Then, add 2ml of hydrazine hydrate (N 2 h 4 ·H 2 0), heated to 60 °C for 2 minutes to allow them to react, then passively cooled to ambient temperature. This reaction leads to Cu 2 O crystals are partially reduced to form Cu / Cu 2 O particles. The resulting Cu / Cu was purified by centrifugation 2 O pellet precipitate, which was washed 3 times with deionized water, and dried under vacuum at 50 °C overnight.
[0047] Analysis of synthesized Cu / Cu by SEM and energy dispersive energy spectroscopy 2 Structural properties of O particles. Figure 6-8 shows Cu / Cu 2 SEM image of O particles, which exhibit a Cu 2 Facets on the rougher surface of the O crystal. Cu / Cu 2 O p...
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