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Test method for evaluating oxidation characteristics of coal CTL base oil

A test method and base oil technology, applied in the directions of flow characteristics, measuring devices, instruments, etc., can solve the problems of inability to widely use industrial production and processing, long test methods, time-consuming and laborious, etc., and achieve shortened test time, high accuracy, The effect of improving accuracy

Inactive Publication Date: 2021-10-29
山西潞安太行润滑科技股份有限公司
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, reasonable test conditions must be selected according to the actual use environment of the lubricating oil to be tested. At present, the commonly used test method is GB / T12581 "Determination of Oxidation Characteristics of Mineral Oil with Inhibitors", but the test method of GB / T12581 takes a long time , is time-consuming and laborious, and cannot be widely used in industrial production and processing. Therefore, we propose a test method for evaluating the oxidation characteristics of coal-based CTL base oils

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  • Test method for evaluating oxidation characteristics of coal CTL base oil

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Embodiment 1

[0034] See figure 1 , A test method for evaluating coal-based CTL base oil oxidation characteristics, including the following steps:

[0035] S1, selected test tube or sample supplies used in coal-based CTL base oil test;

[0036] S2, called the coal-based CTL base oil sample for coal-based CTL base oil test;

[0037] S3, and the viscosity of the coal-based CTL base oil sample before testing, the numerical measure of the acid value, the test before the test is recorded as V1, and the acid value before the test is only T1;

[0038] S4, placed the sampled samples within a dry box that can be operated constant temperature.

[0039] S5, add metal catalyst, organic acid, and hydrogen peroxide, activate the drying box, and constantly warm to 80-150 ° C inside.

[0040] S6, coal-based CTL base oil samples are constantly baking in the drying box, and the reaction time of constant temperature baking is 48-72 hours;

[0041] After the constant temperature bake, the coal-based CTL base oil s...

Embodiment 2

[0058] A test method for evaluating coal-based CTL base oil oxidation characteristics, including the following steps:

[0059] S1, a test tube or a sample article for coal-based CTL base oil test, the test tube or sample article for the test, requires confirmation of the test tube or sample article inside the test, no doped other impurities ;

[0060] S2, 3 sets of coal-based CTL base oil samples for coal-based CTL base oil tests, the coal-based CTL base oil vial amount of coal-based CTL base oil samples is the same;

[0061] S3, and the ratio of motion viscosity before the coal-based CTL base oil sample and the numerical measure of the acid value, the viscosity of the test before the test, and the value of the acid value selected the state of the coal-based CTL base oil at 40 ° C, said Motion viscosity before the test is recorded as V1, and the acid value before the test is t1;

[0062] S4, placed the sampled samples within a dry box that can be operated constant temperature.

[...

Embodiment 3

[0074] A test method for evaluating coal-based CTL base oil oxidation characteristics, including the following steps:

[0075] S1, a test tube or a sample article for coal-based CTL base oil test, the test tube or sample article for the test, requires confirmation of the test tube or sample article inside the test, no doped other impurities ;

[0076] S2, 5 sets of coal-based CTL base oil samples for coal-based CTL base oil tests, the coal-based CTL base oil vials of the coal-based CTL base oil sample were the same;

[0077] S3, and the ratio of motion viscosity before the coal-based CTL base oil sample and the numerical measure of the acid value, the viscosity of the test before the test, and the value of the acid value selected the state of the coal-based CTL base oil at 40 ° C, said Motion viscosity before the test is recorded as V1, and the acid value before the test is t1;

[0078] S4, placed the sampled samples within a dry box that can be operated constant temperature.

[0...

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Abstract

The invention discloses a test method for evaluating the oxidation characteristic of coal CTL base oil, which belongs to the technical field of CTL base oil oxidation characteristic detection. The test method comprises the following steps of S1, selecting a test tube or a sample article for a coal CTL base oil test, S2, weighing a plurality of groups of coal CTL base oil samples for a coal CTL base oil test, and S3, measuring and calculating the values of the kinematic viscosity and the acid value of the coal CTL base oil sample before the test. According to the test method for evaluating the oxidation characteristics of the coal CTL base oil, indirect indexes of the kinematic viscosity and the acid value of oxidation characteristic indexes are determined, the problems that a GB / T12581 test method is long in time and wastes time and labor are solved, and the test result of the oxidation characteristic test of the coal CTL base oil is not influenced, and the average value is obtained by adopting a plurality of test groups, so that the extremely high accuracy of the test data is further ensured.

Description

Technical field [0001] The present invention belongs to the field of CTL base oil oxidation characteristics, and is specifically a test method for evaluating coal-based CTL base oil oxidation characteristics. Background technique [0002] Based on coal-based CTL base oil, oxidation characteristics (oxidative deterministic) refers to the anti-aging properties of oil, which is generally in the precipitate and acid value generated in oil, and is one of the main indicators that determine the life of the oil. Lubricants are in use during use, and they will inevitably contact air, metal and impurities. When used in high temperatures, the oxidation of oil will be accelerated, and the oil produced by the oxidation process will lead to the life of oil and industrial equipment components. Shorten, affect the lubrication effect. At the same time, with the increasingness of energy conservation and environmental regulations, the lubricant products are required to have a longer service life or...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N11/00G01N21/3577
CPCG01N11/00G01N21/3577
Inventor 李树晓郭悦文杜国恩王杰闫强续景郭月芬
Owner 山西潞安太行润滑科技股份有限公司