Electrode paste, and electrode thick film and preparation method thereof
A technology of electrodes and pastes, applied in cable/conductor manufacturing, equipment for manufacturing conductive/semiconductive layers, conductive materials dispersed in non-conductive inorganic materials, etc., can solve the test of adhesion and sulfuration resistance The result is not as expected, the high-frequency conductivity is not as expected, and the price is expensive, etc., to achieve the effect of excellent sintering adhesion
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Embodiment 1
[0030] The preparation of embodiment 1 electrode paste
[0031] First, take Li 2 O, ZnO, Al 2 o 3 、Na 2 O, SrO, V 2 o 5 , B 2 o 3 , SiO 2 Powder, based on the total weight, stirred and mixed according to the following ratio: 0.5-5wt% Li 2 O, 20-50wt% ZnO, 1-5wt% Al 2 o 3 , 1~10wt% Na 2 O, 0.5-5wt% SrO, 1-15wt% V 2 o 5 , 20-50wt% B 2 o 3 , and 1-10wt% SiO 2 .
[0032] The above-mentioned powder is put into the crucible carrier after stirring and mixing, and the powder and the crucible carrier are heated to 1000-1500°C in a resistance furnace for melting for 2 to 4 hours, and then quickly poured into deionized water for extraction to obtain a block of molten glass. Next, the molten glass block is ground for about 24 hours with a coarse grinder, fine grinder, bead mill, etc., to form a powdered glass composition with an average particle size of 1-5 μm, and has a glass softening temperature of 400-900 ° C. point. The so-called average particle size here refers ...
Embodiment 2
[0041] The preparation of embodiment 2 electrode thick film
[0042] Firstly, a ceramic substrate is provided, and the ceramic substrate is obtained by pressing the stacked dielectric sheets and then sintering the dielectric sheets.
[0043] Apply the above-mentioned electrode paste on the end face of the ceramic substrate, then put the ceramic substrate coated with the electrode paste into the electric furnace, and carry out the sintering procedure at a temperature of 850-900°C in an inert gas environment , through the sintering process, the metal powder in the electrode paste will be sintered with each other, and at the same time, the organic binder, solvent and other components in the electrode paste will be burned off, and then a thick electrode film with a conductive pattern will be obtained. The formed electrode The thick film has extremely high electrical conductivity and is excellent in electromigration resistance, solder heat resistance, and adhesion to ceramic substr...
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