High-heat-resistance and anti-red-storm infrared optical composite material composition and preparation method thereof
A technology of infrared optics and composite materials, which is applied in the protection field of composite material compositions, can solve the problems of being susceptible to interference, light source red exposure, easy aging and heat resistance, etc., and achieves the effect of strong anti-interference ability.
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[0062] Another embodiment of the present invention provides a method for preparing a high heat-resistant red exposure-proof infrared-transmitting optical composite material composition, comprising the following steps:
[0063] S1: Weigh the PMMA resin, heat-resistant agent, antioxidant, diffusing powder, ultraviolet absorber, light stabilizer and infrared penetrating agent in proportion, then put it into a high-speed mixer and stir it for 20-30 minutes to form a mixture , the rotating speed of the high-speed mixer is 190-230 rev / min;
[0064] S2: Put the mixture into the twin-screw extruder, and after melting, extruding, granulating and drying, the finished product is obtained. The extruder includes nine processing zones, and the processing temperature of each processing zone is 180- 200°C, the vacuum degree of the extruder is ≥0.09MPa, the aspect ratio of the extruder is 30-38, and the screw speed of the extruder is 320-580 rpm;
[0065] S3: Cut into granules by high-speed g...
Embodiment 1
[0067] PMMA resin: 79 parts, heat-resistant agent: 2.1 parts, antioxidant: 2.1 parts, diffusion powder 1.6 parts, ultraviolet absorber 6.7 parts, light stabilizer: 1 part, infrared penetrating agent: 13.4 parts, mix at high speed The above components are mixed evenly in the machine at room temperature, and then produced in a twin-screw extruder; processing conditions: material mixing speed: 190 rpm; temperature in zone one: 180°C, temperature in zone two: 185°C, temperature in zone three Zone temperature: 190°C, Zone 4 temperature: 195°C, Zone 5 temperature: 200°C, Zone 6 temperature: 200°C, Zone 7 temperature: 195°C, Zone 8 temperature: 195°C, Zone 9 temperature: 200°C, screw speed : 400 rpm, the vacuum degree of the extruder is 0.09MPa, and the aspect ratio of the extruder is 30.
Embodiment 2
[0069] PMMA resin: 77 parts, heat-resistant agent: 0.9 part, antioxidant: 0.9 part, diffusing powder 0.6 part, ultraviolet absorber 8.25 part, light stabilizer: 1.8 part, infrared penetrating agent: 16.5 part, mix at high speed The above components are mixed evenly in the machine at room temperature, and then produced in a twin-screw extruder; processing conditions: material mixing speed: 190 rpm; temperature in zone one: 180°C, temperature in zone two: 185°C, temperature in zone three Zone temperature: 190°C, Zone 4 temperature: 195°C, Zone 5 temperature: 200°C, Zone 6 temperature: 200°C, Zone 7 temperature: 195°C, Zone 8 temperature: 195°C, Zone 9 temperature: 200°C, screw speed : 400 rpm, the vacuum degree of the extruder is 0.11MPa, and the aspect ratio of the extruder is 34.
[0070] In summary, the heat-resistant temperature of the composite material obtained in the present invention reaches 120 degrees, and the composite infrared optical sky eye material has a higher in...
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Abstract
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