High-strength temporary plugging agent capable of realizing well zone seepage and preparation method thereof
A high-strength, temporary plugging agent technology, applied in the direction of chemical instruments and methods, drilling compositions, etc., to achieve the effect of firm plugging and less residual gel
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Embodiment 1
[0028] Take 600g of water and 400g of acetone to make a solvent, take 1g of hydrophilic nano silicon dioxide and evenly disperse in 1000g of solvent, then add 40g of glycerol allyl ether, after ultrasonication for 40min, add 80g of acrylamide, stir to dissolve, Under the condition of stirring and continuous nitrogen flow, add 0.16g N,N-methylene acrylamide, 1.6g butanediol diacrylate and 0.84g potassium persulfate, and continue to react at 65°C for 8h, the reaction is over Finally, the product was rotary evaporated to dryness at 60°C, and then crushed, sieved, and then dried to obtain the high-strength temporary plugging agent G1 that can realize seepage in the well zone.
Embodiment 2
[0030] Take 600g of water and 400g of acetone to make a solvent, take 1g of hydrophilic nano-calcium carbonate and disperse evenly in 1000g of solvent, then add 45g of glycerin allyl ether, after ultrasonication for 40min, add 50g of acrylamide and 40g of acrylic acid, stir to dissolve , under the condition of stirring and continuous nitrogen flow, add 0.16g N,N-methylene acrylamide, 1.6g butanediol diacrylate and 0.84g potassium persulfate, and continue to react at 65°C for 8h, After the reaction, the product was rotary evaporated to dryness at 60°C, and then crushed, sieved, and then dried to obtain the high-strength temporary plugging agent G2 that can realize seepage in the well zone.
Embodiment 3
[0032] Take 550g of water and 450g of acetone to make a solvent, take 1.5g of hydrophilic nano-silica and disperse evenly in 1000g of solvent, then add 35g of glycerin allyl ether, after ultrasonication for 40min, add 50g of acrylamide and 40g of methacrylamide , stirred to dissolve, and under the condition of stirring and continuing to blow nitrogen, 0.16g of N,N-methylene acrylamide, 1.6g of dipropylene glycol diacrylate and 0.84g of azobisisobutylamidine hydrochloride were added, And continue to react at a temperature of 53°C for 8 hours. After the reaction is completed, the product is evaporated to dryness at 60°C, and then crushed, sieved, and dried again to obtain a high-strength temporary plugging agent that can realize seepage in the well zone G3.
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