Temporary plugging agent capable of realizing well zone seepage and preparation method thereof
A temporary plugging agent and percolation technology, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., to achieve the effects of firm plugging, less residual gel, and improved adsorption
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Embodiment 1
[0021] Take 500g of water and 500g of acetone as the solvent, take 80g of acrylamide and 35g of glycerol allyl ether into the above-mentioned solvent, stir to dissolve, continue to pass nitrogen gas to discharge the air in the system and keep stirring, and then add 0.16g N, N-methylene acrylamide, 1.6g dipropylene glycol acrylate, 0.92g potassium persulfate, reacted at 65°C for 10h, after the reaction, the product was rotary evaporated to dryness at 60°C, and then It is pulverized, sieved, and then dried to obtain the temporary plugging agent T1.
Embodiment 2
[0023] Take 500g of water and 500g of acetone as the solvent, take 90g of acrylamide and 45g of glycerol allyl ether into the above-mentioned solvent, stir to dissolve, continue to pass nitrogen gas to discharge the air in the system and keep stirring, and then add 0.11g N,N-methylene acrylamide, 1.2g of butanediol diacrylate, 0.92g of potassium persulfate were reacted for 10 hours at a temperature of 65°C. After the reaction, the product was rotary evaporated to dryness at 60°C. Then crush it, sieve it, and then dry it to get the temporary plugging agent T2.
Embodiment 3
[0025] Take 400g of water and 600g of acetone as the solvent, take 50g of acrylamide, 35g of acrylic acid, and 45g of glycerol allyl ether into the aforementioned solvent, stir to dissolve, continue to pass nitrogen into the system to discharge the air and keep stirring, and then Add 0.11g of N,N-methylene acrylamide, 1.2g of dipropylene glycol acrylate, 0.92g of azobisisobutylamidine hydrochloride, and react at a temperature of 53°C for 8h. The product was rotary evaporated to dryness, then crushed, sieved, and then dried to obtain the temporary blocking agent T3.
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