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Temporary plugging agent capable of realizing well zone seepage and preparation method thereof

A temporary plugging agent and percolation technology, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., to achieve the effects of firm plugging, less residual gel, and improved adsorption

Active Publication Date: 2022-02-15
西安维克特睿油气技术有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] At present, under the pressure of environmental protection, some fracturing processes consider directly retaining the fracturing fluid in the reservoir to achieve the effect of reducing flowback or zero flowback. , the braising time usually ranges from a few days to tens of days, therefore, the conventional temporary plugging agent cannot meet these requirements, and there is an urgent need for a temporary plugging agent with a controllable plugging removal time and a long plugging removal time

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] Take 500g of water and 500g of acetone as the solvent, take 80g of acrylamide and 35g of glycerol allyl ether into the above-mentioned solvent, stir to dissolve, continue to pass nitrogen gas to discharge the air in the system and keep stirring, and then add 0.16g N, N-methylene acrylamide, 1.6g dipropylene glycol acrylate, 0.92g potassium persulfate, reacted at 65°C for 10h, after the reaction, the product was rotary evaporated to dryness at 60°C, and then It is pulverized, sieved, and then dried to obtain the temporary plugging agent T1.

Embodiment 2

[0023] Take 500g of water and 500g of acetone as the solvent, take 90g of acrylamide and 45g of glycerol allyl ether into the above-mentioned solvent, stir to dissolve, continue to pass nitrogen gas to discharge the air in the system and keep stirring, and then add 0.11g N,N-methylene acrylamide, 1.2g of butanediol diacrylate, 0.92g of potassium persulfate were reacted for 10 hours at a temperature of 65°C. After the reaction, the product was rotary evaporated to dryness at 60°C. Then crush it, sieve it, and then dry it to get the temporary plugging agent T2.

Embodiment 3

[0025] Take 400g of water and 600g of acetone as the solvent, take 50g of acrylamide, 35g of acrylic acid, and 45g of glycerol allyl ether into the aforementioned solvent, stir to dissolve, continue to pass nitrogen into the system to discharge the air and keep stirring, and then Add 0.11g of N,N-methylene acrylamide, 1.2g of dipropylene glycol acrylate, 0.92g of azobisisobutylamidine hydrochloride, and react at a temperature of 53°C for 8h. The product was rotary evaporated to dryness, then crushed, sieved, and then dried to obtain the temporary blocking agent T3.

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Abstract

The invention provides a temporary plugging agent capable of realizing well zone seepage and a preparation method thereof. The temporary plugging agent is prepared by the following steps: dissolving an acrylamide monomer and a glyceryl allyl ether monomer in a solvent, adding N,N-methylene acrylamide, an acrylate compound, and an initiator, continuously reacting for 5-12 hours, and after reaction, drying to obtain thetemporary plugging agent, wherein the acrylate compound is one of butanediol diacrylate, dipropylene glycol acrylate and neopentyl glycol diacrylate, the mass ratio of N,N-methylene acrylamide to the acrylate compound is 1: (5-12), and the mass of N,N-methylene acrylamide accounts for 0.08%-0.15% of the total mass of the monomer. According to the temporary plugging agent, the plugging rate is high and can reach 95% or above, the plug removal rate is high and can reach 82% or above, residual gel obtained after plug removal is conducted finally is little, the influence on the stratum is small, and the temporary plugging agent can be used for well zone seepage volume fracturing.

Description

technical field [0001] The invention belongs to the technical field of oil recovery additives, and in particular relates to a temporary plugging agent capable of realizing seepage in well zones and a method for preparing the temporary plugging agent. Background technique [0002] With the development of old oil wells in major oilfields across the country, the production of oil wells has gradually decreased. Practical fracturing means to increase oil and gas production and prolong the life of oil wells is a common method at present. Before the fracturing operation, it is first necessary to use a temporary plugging agent to seal the original fractures. After the fracturing operation is completed, the temporary plugging agent will gradually remove the plugging, which can avoid the damage of the plugging agent to the formation. [0003] Well zone seepage volume fracturing is a relatively new fracturing idea proposed at present, which specifically refers to the fracturing mode th...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08F220/56C08F216/14C08F222/38C08F222/14C08F222/20C08F220/06C09K8/512C09K8/88
CPCC08F220/56C09K8/512C09K8/887C08F216/1416C08F222/385C08F222/102C08F220/06Y02P20/141
Inventor 安耀清时际明蔡为立于思想王志兴
Owner 西安维克特睿油气技术有限公司
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