Process for preparing white cross-linked protein powder from silkworm pupa

A manufacturing process and protein separation technology, applied in the field of silkworm chrysalis protein manufacturing process, can solve the problems of not being able to use light-colored fabrics, uneconomical, and solvent oil consumption, and achieve the effects of environmental protection, low production costs, and high product quality

Inactive Publication Date: 2003-02-19
CHONGQING UNIV
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  • Application Information

AI Technical Summary

Problems solved by technology

[0005] 3. Due to the drying method used in this process, the dried product is in the form of lumps, and after being crushed, it becomes black particles, which need to be soaked and softened for a long time to dissolve, and the silk made of this protein is yellowish brown, which cannot be used for light colors. fabric;
[0006] 4. Since this manufacturing process has no separation and removal of residual fat except for the degreasing of silkworm chrysalis, this process is only suitable for dried silkworm chrysalis with a very low fat content (≤1%), not for those with a fat content higher than 3%. Silkworm chrysalis (the fat content of commercially available defatted silkworm chrysalis ≥ 3%)
If this process is used to process the commercially available defatted silkworm chrysalis and the silkworm chrysalis protein is used for spinning, it is easy to block the filter cloth when filtering, and it is easy to block the silk holes when spinning; when it is used in the food industry and animal feed, it is easy to become rancid and produce unpleasant smell. Odor, affecting food quality and appetite
In fact, when the fat content of dried silkworm chrysalis drops to about 3%, reducing its fat content will consume a large amount of solvent oil, and the efficiency is extremely low, which is very uneconomical

Method used

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Embodiment Construction

[0018] Below in conjunction with embodiment, further illustrate the present invention.

[0019] Dissolve the defatted silkworm chrysalis powder in a dilute NaOH solution of 10 times the concentration of 0.5% at a high temperature of 80°C to dissolve the protein and saponify the oil. The dissolving and saponification time is 5 hours, and after 5 hours, use a horizontal spiral centrifuge to separate the silkworm chrysalis protein liquid Chitin and saponified oil particles in the chrysalis, and then use a disc separator to separate the residual and unsaponified oil in the silkworm chrysalis isolated protein solution, and then use sulfuric acid to decolorize the low-fat silkworm chrysalis isolated protein solution at a low temperature of 50 ° C. Adjust the isoelectric point, control its pH value to 4, and precipitate, then use a horizontal screw centrifuge to separate the precipitated silkworm chrysalis protein isolate, wash 2 times with 20 times of pure water, and then precipitate...

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Abstract

A process for preparing non-odour white silkworm pupa protein from the degreased silkworm pupa powder includes dissolving saponizing, separation, regulating isopotential point, separating, washing, deodouring and cross-linking. Its advantages are high extracting rate, and high quality of product.

Description

1. Technical field [0001] The invention belongs to the technical field of silkworm chrysalis protein manufacturing technology. 2. Technical Background [0002] Silkworm chrysalis is one of the main by-products of the silk reeling industry. Silkworm chrysalis is rich in protein with high nutritional value. Silkworm chrysalis protein is widely used in food industry and animal feed. . For example, the process for extracting silkworm chrysalis disclosed in "a spinning solution containing silkworm chrysalis protein" in the patent No. ZL 95111330.5 is to dry, degrease, soak, and dissolve fresh silkworm chrysalis in an alkaline solution. Finally, it is filtered, molecular sieve is used to control the molecular weight, and then decolorized to adjust the isoelectric point, washed with water, and finally dehydrated and dried to obtain silkworm chrysalis protein. This manufacturing process has the following disadvantages: [0003] 1. Extract protein from the complete silkworm chrysa...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23J1/00
Inventor 周小华
Owner CHONGQING UNIV
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