Ultralow dielectric constant layer with controlled biaxial stress
a dielectric constant and controllable technology, applied in plasma technology, transportation and packaging, energy-based chemical/physical/physico-chemical processes, etc., can solve the problems of increasing signal delay in ulsi electronic devices, tendency to crack, etc., to reduce the biaxial stress, control the biaxial stress, the effect of low and controllable biaxial stress
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example 1
[0059]In this example, two types of SiCOH films were deposited on Si wafers. The first type of SiCOH film was an ultra-low k dielectric film deposited by means of PECVD, and which in as-deposited state contained a matrix based on the precursor diethoxymethylsilane (DEMS) and an organic phase that can later be removed by means of an energy source to stabilize the film and improve its properties (electrical, mechanical, adhesive), resulting in a final optimum film. Suitable energy sources include thermal, chemical, ultraviolet (UV) light, EB, RF, microwave, and plasma. Combinations of the aforementioned energy sources can also be used in the present invention. Within the present invention, the ambient for thermal, UV, EB, laser, or RF treatment is done in an environment comprising an inert gas such as N2, H2, Ar, He, Xe, or other noble gas or a hydrocarbon gas or a mixture thereof and containing a concentration of O2 in the range from 0 to 10 ppm.
[0060]The second type of SiCOH film wa...
example 2
[0111]In this example, a specific composition of an ultra-low k SiCOH film was deposited on Si wafers by means of PECVD. In the as-deposited state these SiCOH films contained a matrix based on the precursor DEMS and an organic phase that was later removed by means of UV light exposure at elevated temperature to stabilize the SiCOH film and improve its properties (electrical, mechanical, adhesive), resulting in a final optimum SiCOH film on the Si wafers.
[0112]The SiCOH film on respective Si wafers were UV cured, treated or annealed in three different gas environments. The three different gas environments were: a noble gas such as He or Ar, He mixed with H2, and O2. For the UV treatments, the substrate temperature was maintained for 20 minutes at 400° C. during the treatment, and the same UV lamp was used for the UV treatments.
[0113]FIG. 13, shows the biaxial stress of a SiCOH film on a Si wafer after UV treatment. In FIG. 13, the ordinate represents biaxial stress and the abscissa r...
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