Ink jet faceplate coatings comprising structured organic films
a structured organic film and ink jet technology, applied in the field of coatings for the front face of ink jet printheads, can solve the problems of degrading print quality, affecting the quality of printed materials, so as to prevent ink contamination, prevent ink contamination, and reduce the effect of adhesion
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example 1
[0180](Action A) Preparation of the liquid containing reaction mixture. The following were combined: the building block N,N,N′,N′-tetrakis-[(4-hydroxymethyl)phenyl]-biphenyl-4,4′-diamine (2.64 g); the building block N,N′-bis-(3-hydroxyphenyl)-N,N′-diphenyl-biphenyl-4,4′-diamine (3.73 g); the additive Cymel 303 (67 mg), the additive Silclean 3700 (264 mg), the catalyst Nacure 5225 (132 mg) and Dowanol (18.48 g). The mixture was shaken and heated to 55° C. for 60 minutes. Upon cooling to room temperature, the solution was filtered through a five micron PTFE membrane.
[0181](Action B) Deposition of reaction mixture as a wet film. The reaction mixture was applied to a substrate (either polyimide or stainless steel sheets) using a constant velocity draw-down coater outfitted with a bird bar having a 2 mil gap.
[0182](Action C) Promotion of the change of the wet film to a dry SOF. The substrate (polyimide and stainless steel sheets) supporting the wet layer was rapidly transferred to an act...
example 2
[0183](Action A) Preparation of the liquid containing reaction mixture. The following were combined: the building block octafluoro-1,6-hexanediol [segment=octafluoro-1,6-hexyl; Fg=hydroxyl (—OH); (0.43 g, 1.65 mmol)], a second building block N4,N4,N4′,N4′-tetrakis(4-(methoxymethyl)phenyl)biphenyl-4,4′-diamine [segment=N4,N4,N4′,N4]-tetra-p-tolylbiphenyl-4,4′-diamine; Fg=methoxy ether (—OCH3); (0.55 g, 0.82 mmol)], an acid catalyst delivered as 0.05 g of a 20 wt % solution of Nacure XP-357 to yield the liquid containing reaction mixture, a leveling additive delivered as 0.04 g of a 25 wt % solution of Silclean 3700, and 2.96 g of 1-methoxy-2-propanol. The mixture was shaken and heated at 85° C. for 2.5 hours, and was then filtered through a 0.45 micron PTFE membrane.
[0184](Action B) Deposition of reaction mixture as a wet film. The reaction mixture was applied to the reflective side of a metalized (TiZr) MYLAR™ substrate using a constant velocity draw down coater outfitted with a bir...
example 3
[0186](Action A) Preparation of the liquid containing reaction mixture. The following were combined: the building block dodecafluoro-1,8-octanediol [segment=dodecafluoro-1,8-octyl; Fg=hydroxyl (—OH); (0.51 g, 1.41 mmol)], a second building block N4,N4,N4′,N4′-tetrakis(4-(methoxymethyl)phenyl)biphenyl-4,4′-diamine [segment=N4,N4,N4′,N4′-tetra-p-tolylbiphenyl-4,4′-diamine; Fg=methoxy ether (—OCH3); (0.47 g, 0.71 mmol)], an acid catalyst delivered as 0.05 g of a 20 wt % solution of Nacure XP-357 to yield the liquid containing reaction mixture, a leveling additive delivered as 0.04 g of a 25 wt % solution of Silclean 3700, and 2.96 g of 1-methoxy-2-propanol. The mixture was shaken and heated at 85° C. for 2.5 hours, and was then filtered through a 0.45 micron PTFE membrane.
[0187](Action B) Deposition of reaction mixture as a wet film. The reaction mixture was applied to the reflective side of a metalized (TiZr) MYLAR™ substrate using a constant velocity draw down coater outfitted with a...
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