Extraction of garlic volatile oil
A garlic oil and volatile oil technology, applied in fermentation, pharmaceutical formulations, fat oil/fat production, etc., can solve the problems of adjusting DADS and DATS, waste of manpower and material resources, and no explanation, and achieve the effect of shortening working hours, saving energy and saving time.
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Embodiment 1
[0066] Anhui Hefei garlic 2800g, crush the garlic into 3~5mm particles in a masher, add 5 times the amount of water, 50℃ enzymatic hydrolysis for 1 hour, extract garlic volatile oil for 1 hour, the volatile oil is dehydrated by anhydrous sodium sulfate, the oil yield rate It is 0.25%, the content of diallyl trisulfide (DATS) in garlic oil is 35.65%, the content of diallyl disulfide (DADS) is 18.20%, diallyl trisulfide (DATS) and diallyl The total content of disulfide (DADS) is 53.85%.
Embodiment 2
[0068] Shandong Jinxiang garlic 1500g, cut into 1~2mm garlic slices, add 5 times the amount of water, 50℃ enzymatic hydrolysis for 1.5 hours, extract garlic volatile oil for 1 hour, after the volatile oil is dehydrated by anhydrous sodium sulfate, the oil yield is 0.283%. The content of diallyl trisulfide (DATS) in garlic oil is 30.81%, the content of diallyl disulfide (DADS) is 27.94%, diallyl trisulfide (DATS) and diallyl disulfide (DADS) The total content is 58.75%.
Embodiment 3
[0070] Shandong Cangshan garlic 1600g, crush the garlic into 3~5mm particles in a masher, add 6 times the amount of water, enzymatically hydrolyze at 55℃ for 1 hour, extract garlic volatile oil for 1 hour, the volatile oil is dehydrated by color-changing silica gel, the oil yield is 0.34 %, the content of diallyl trisulfide (DATS) in garlic oil is 44.47%, the content of diallyl disulfide (DADS) is 17.33%, diallyl trisulfide (DATS) and diallyl disulfide are determined (DADS) total content is 61.80%.
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