Reagent kit for detecting early stage cancer
An early detection and kit technology, applied in the fields of medicine and pharmacy, can solve the problems of inconvenient promotion, high detection cost, and inconvenient use, and achieve the effects of easy promotion, low cost, and easy acquisition.
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[0015] 1. Separation and extraction of L-fucose dehydrogenase
[0016] Extract L-fucose dehydrogenase from fresh pork liver: Homogenize 250 grams of fresh pork liver with a tissue masher, then add 1L 0.25mol / L sucrose, centrifuge at 25000g for 20min, discard the precipitate and take the supernatant, add 450ml to saturate Ammonium sulfate, centrifuge at 25000g for 20min after standing for 15min, discard the precipitate and take the supernatant, add 400ml saturated ammonium sulfate, centrifuge at 25000g for 20min after standing for 15min, discard the supernatant to remove the precipitate, dialyze with 0.005M phosphate buffer saline (PBS), and take the dialysate Diethylaminoethyl (DEAE) cellulose column (DE 52 ), eluted with a gradient of 0.005mol / L phosphate buffered saline (PBS) containing 0.05-0.15mol / L sodium chloride (NaCl), and collected the eluted fraction of 0.1-0.15mol / L sodium chloride (NaCl) Concentrate, measure L-fucose dehydrogenase, and store in a -70°C refrigerato...
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