Process for smelting cleaning titan and titan alloy casting ingot

A titanium alloy and ingot casting technology, which is applied in the smelting field of clean titanium and titanium alloy ingots, can solve problems such as economic loss, high titanium alloy clutter, component fatigue failure, etc., achieve uniform chemical composition and reduce production costs

A titanium alloy and ingot casting technology, which is applied in the smelting field of clean titanium and titanium alloy ingots, can solve problems such as economic loss, high titanium alloy clutter, component fatigue failure, etc., achieve uniform chemical composition and reduce production costs

CN101307398AInactive Publication Date: 2008-11-19NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0009] Smelting of industrial pure titanium TA2: Weigh 20kg of first-grade sponge titanium, press the first-grade sponge titanium into an electrode block, the electrode block weighs 20kg, weld the pressed electrode block into an electrode, and the electrode length is about 1500mm. The electrode is smelted into a Ф215mm ingot on the electron beam cooling bed melting furnace at one time, and the smelting vacuum degree is lower than 6×10 -2 Pa, the melting speed is 100kg / h, and the melting power is 200kW. The surface of the titanium ingot obtained by smelting is smooth and clean, without subcutaneous pores, cold shuts, etc. The solidification structure of titanium ingot is very good. The titanium ingot was forged into a Ф30mm bar, the surface was polished, and no TiN and WC inclusions were found through the ultrasonic flaw detection of the 0.8mm flat-bottomed hole.

Embodiment 2

[0011] Melting of TC4 alloy: According to the alloy composition requirements, weigh 1.356kg of Al-V master alloy, 0.918kg of Al bean, and 17.726kg of sponge titanium, mix the sponge titanium, Al-V master alloy and Al bean, and press it into an electrode block. The single weight of the electrode block is 20kg, and the pressed electrode block is welded into an electrode, and the length of the electrode is about 1500mm. The electrode is smelted into a Ф215mm titanium alloy ingot on the electron beam cooling bed melting furnace at one time, and the smelting vacuum degree is lower than 6×10 -2 Pa, the melting speed is 70kg / h, and the melting power is 180kW. The surface of the titanium alloy ingot is smooth and clean, without subcutaneous pores, cold shuts, etc. The solidification structure of titanium alloy ingot is very good, the center is equiaxed crystal, and the outer part is columnar crystal. The chemical composition is uniform. Titanium alloy ingots were forged into Ф30mm ...

Embodiment 3

[0013] Melting of TC11: According to the alloy composition requirements, weigh 0.712kg of Al beans, 1.078kg of Al-Mo master alloy, 0.513kg of Al-Si master alloy, 0.30kg of sponge zirconium, and 17.397kg of sponge titanium, and press them into electrode blocks after mixing. The single weight of the block is 20kg, and the pressed electrode block is welded into an electrode, and the length of the electrode is about 1500mm. The electrode is smelted into a Ф215mm titanium alloy ingot on the electron beam cooling bed melting furnace at one time, and the smelting vacuum degree is lower than 6×10 -2 Pa, the melting speed is 150kg / h, and the melting power is 300kW. The surface of the titanium alloy ingot is smooth and clean, without subcutaneous pores, cold shuts, etc. The solidification structure of titanium alloy ingot is very good, the center is equiaxed crystal, and the outer part is columnar crystal. The chemical composition is uniform. Titanium alloy ingots were forged into Ф3...

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Abstract

The invention discloses a method for melting a clean titanium ingot and a titanium alloy ingot. The method comprises the following steps of: weighing sponge titanium or weighing a pure alloy addition element, an intermediate alloy and sponge titanium; pressing the sponge titanium or the mixed pure alloy addition element, the intermediate alloy and the sponge titanium into an electrode block; soldering the pressed electrode block into an electrode; and performing primary electron-beam cold-hearth melting to the electrode by an electron-beam cold-hearth furnace to produce a titanium ingot or a titanium alloy ingot which are clean and have homogeneous chemical compositions. The melting vacuity for the electron-beam cold-hearth melting is lower than 6x10<-2>Pa, the melting speed for the electron-beam cold-hearth melting is between 70 and 150kg / h, and the melting power for the electron-beam cold-hearth melting is between 100 and 300kW; and the weight of the pure alloy addition elements and the intermediate alloys is 0 to 20 percent of the total weight of the titanium alloy ingot. The titanium ingot and the titanium alloy ingot produced by the method have homogeneous chemical compositions, and macrostructures of the ingots are superior to a vacuum consumable arc-melted ingot without TiN, WC and other high melting-point inclusions.

Description

technical field [0001] The invention relates to a method for smelting clean titanium and titanium alloy ingots, belonging to the technical field of titanium alloy smelting. Background technique [0002] Titanium alloys are widely used in aviation, aerospace and other fields due to their high specific strength, corrosion resistance, and high temperature resistance. Most titanium and titanium alloy parts are made of sponge titanium or pure alloys, adding elements, intermediate alloys and sponge titanium to press the electrode block, then welding the electrode block into an electrode, melting it into an ingot by vacuum consumable arc, and improving the structure and properties by forging. processed. The main production method of sponge titanium is the Kroll method. In the process of magnesium reduction and vacuum distillation, due to the possible air leakage and pollution, there are inevitably nitrogen-rich inclusions in the produced sponge titanium. In the subsequent crushing...

Claims

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Application Information

Patent Timeline
19 Nov 2008
Publication
CN101307398A
IPC
C22C1/02; C22C14/00
Inventors
张英明; 韩明臣