Petroleum ether extracted yellow tea extract, preparation and application thereof
A technology of petroleum ether extraction and petroleum ether, which is applied in the field of tobacco additive preparation to achieve the effect of enriching cigarette aroma, reducing irritation and miscellaneous gas, and improving aftertaste
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Embodiment 1
[0028] Weigh 500 grams of yellow tea with an electronic balance, put it into a flask, add 2500ml of medical grade petroleum ether with a boiling point of 30-60°C, soak for 10h at 20°C, separate the solid and liquid with a Bush funnel, collect the clear liquid, and get The liquid was distilled and concentrated for 2.0 h at a vacuum degree of 0.05 MPa and a distillation temperature of 28° C., and the solvent was removed to obtain 0.6 g of extract.
Embodiment 2
[0030] Weigh 1,000 grams of yellow tea with an electronic balance, put it into an Erlenmeyer flask, add 10,000ml of petroleum ether with a boiling point of 60-90°C, soak for 20 hours at 30°C, separate the solid and liquid with a Bush funnel, collect the clear liquid, and obtain the liquid Distill and concentrate for 1.0 h at a vacuum of 0.1 MPa and a distillation temperature of 30° C., and remove the solvent to obtain 2.45 g of extract.
Embodiment 3
[0032] Weigh 1000 grams of yellow tea with an electronic balance, put it into an Erlenmeyer flask, add 15000ml of petroleum ether with a boiling point of 30-60°C, soak for 10 hours at 15°C, separate the solid and liquid with a Bush funnel, collect the clear liquid, and obtain the liquid Distill and concentrate for 1.5 h under the condition of vacuum degree of 0.01 MPa and distillation temperature of 25° C., and remove the solvent to obtain 2.50 g of extract.
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