Dental adhesive capable of resisting fretting damage, method for preparing same and application thereof
An adhesive and dental technology, applied in dental preparations, dentistry, dental prosthesis, etc., can solve problems affecting the service life of fixed restorations, affecting the long-term stability of dental crowns, and increasing the workload of doctors, achieving good microscopic Effects of reducing damage due to vibration, reducing work load, and increasing service life
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Embodiment 1-4
[0019] The specific implementation manner of embodiment 1-4 is:
[0020] A dental adhesive is composed of a powder and a liquid, wherein the components and mass ratio of the powder are 90-95 parts of zinc oxide, 2 parts of aluminum oxide and 3 parts of bismuth oxide; the components and mass ratio of the liquid are The ratio is 74-76 parts of orthophosphoric acid, 2 parts of zinc oxide, and 22-24 parts of deionized water.
[0021] The method for preparing the above-mentioned dental adhesive is as follows: take the zinc oxide, aluminum oxide and bismuth oxide in the mass ratio, and mix them fully to obtain a powder; weigh the orthophosphoric acid, desulfurized Ionized water and zinc oxide, then phosphoric acid is added to the ionized water, and then zinc oxide is added to the solution to make a liquid.
[0022] The use of the above-mentioned dental adhesive is as follows: After mixing 1.6-1.8 grams of powder with 1 milliliter of liquid evenly, it is used for bonding dental rest...
Embodiment 5
[0028] This example is substantially the same as Example 1, except that an appropriate amount of pigment is also added in the powder. The amount of trace pigment added is to make the color of the adhesive distinguishable from other dental adhesives. The powder of this example also contains an acid-base indicator whose discoloration point is a neutral point, that is, the pH value corresponding to the discoloration point is 6.7-7.2. The acid-base indicator can indicate the end point of the chemical reaction of the reconciled powder and liquid. Various commercially available existing acid-base indicators whose discoloration points are neutral points, such as phenolphthalein, methyl orange, and litmus, can be used; of course, the amount used is also based on the color of the acid-base indicator that can be observed.
[0029] After testing, the physical and chemical properties of the adhesive of the present invention after curing are shown in the following table:
[0030] ...
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