Manufacture method of solar silicon single crystal
A production method, silicon single crystal technology, applied in the direction of single crystal growth, single crystal growth, chemical instruments and methods, etc., can solve problems such as unusable, rising production costs, and inability to form crystals, so as to reduce production costs and improve enterprise efficiency. Economic benefit, waste reduction effect
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Embodiment 1
[0031] A method for manufacturing solar silicon single crystals, using waste polysilicon leftovers as main raw materials to prepare solar silicon single crystals, the manufacturing method comprising the following steps:
[0032] The first step: first classify the polysilicon waste:
[0033] (1) Place the head and tail material, crucible bottom material and waste sheet material of polysilicon leftovers respectively,
[0034] (2) The above-mentioned head and tail materials, crucible bottom materials, and waste sheet materials are all selected from N-type polysilicon scraps with a resistivity of 0.3Ω.cm,
[0035] (3) cleaning and drying: the head and tail material, crucible bottom material, and waste sheet material are cleaned with acidic solution respectively, and then dried; the acidic solution used is mixed by concentration of 40% hydrofluoric acid and concentration of 65% nitric acid, Wherein the weight ratio of hydrofluoric acid and nitric acid is 1: 5;
[0036] A. Head an...
Embodiment 2
[0062] A method for manufacturing solar silicon single crystals, using waste polysilicon leftovers as main raw materials to prepare solar silicon single crystals, the manufacturing method comprising the following steps:
[0063] The first step: first classify the polysilicon waste:
[0064] (1) Place the head and tail material, crucible bottom material and waste sheet material of polysilicon leftovers respectively,
[0065] (2) The above-mentioned head and tail materials, crucible bottom materials, and waste sheet materials are all selected from N-type polysilicon scraps with a resistivity of 1Ω.cm,
[0066] (3) cleaning and drying: the head and tail material, crucible bottom material, and waste sheet material are cleaned with acidic solution respectively, and then dried; the acidic solution used is mixed by concentration of 42% hydrofluoric acid and concentration of 66% nitric acid, Wherein the weight percent of hydrofluoric acid and nitric acid is 1: 5;
[0067]A. Head and...
Embodiment 3
[0079] A method for manufacturing solar silicon single crystals, using waste polysilicon leftovers as main raw materials to prepare solar silicon single crystals, the manufacturing method comprising the following steps:
[0080] The first step: first classify the polysilicon waste:
[0081] (1) Place the head and tail material, crucible bottom material and waste sheet material of polysilicon leftovers respectively,
[0082] (2) The above-mentioned head and tail material, crucible bottom material, and waste sheet material are all selected N-type polysilicon scraps with a resistivity of 2Ω.cm,
[0083] (3) cleaning and drying: the head and tail material, crucible bottom material, and waste sheet material are cleaned with acidic solution respectively, and then dried; the acidic solution used is mixed by concentration of 43% hydrofluoric acid and concentration of 67% nitric acid, Wherein the weight ratio of hydrofluoric acid and nitric acid is 1: 5.5;
[0084] A. Head and tail m...
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