Preparation method of thermoplastic polyimide-based composite material structure member (cover)
A technology of polyimide-based and composite materials, which is applied in the field of preparing skin components from resin-based composite materials, and can solve problems such as difficulty in preparing high-density products, difficulty in removing solvents from small molecules, and high manufacturing costs. , to achieve the effect of low manufacturing cost, short molding cycle and good toughness
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Embodiment 1
[0024] At 100g / m 2 Spread 2 0.001mm thermoplastic polyimide films on top and bottom of T300 carbon fiber 1k plain cloth, fiber / film=80 / 20. For 2mm thick parts, 14 layers are required. Thermoplastic polyimide film and carbon fiber and glass fiber braid layer are layered in turn. Put the layered carbon fiber (carbon cloth) and thermoplastic polyimide film into the skin part of the mold cavity of the cover part, and add the thermoplastic polyimide-based chopped fiber to the mold cavity reinforcement part Composite material NDJ-901-C30 powder (30% chopped carbon fiber content, 0.05mm fiber length), mold clamping. After heating in a mold press at 400°C for 0.5 hours, pressurize it at a pressure of 100MPa for 5 minutes, and cool to 200°C for demolding. The density of the cover can be 1600kg / m 3 , The tensile strength is 800MPa, and the total molding time is 35 minutes.
Embodiment 2
[0026] The glass cloth can be SW280-100 of Nanjing Fiberglass Research and Design Institute. At 400g / m 2 Spread one piece of 0.250mm thermoplastic polyimide film on and between the bottom of the glass cloth, fiber / film=20 / 80. For 2mm thick parts, 7 layers are required. The film and the carbon fiber and glass fiber braid are layered in turn. Put the layered glass cloth and thermoplastic polyimide film mixture into the skin part of the part mold cavity, and add the thermoplastic polyimide-based chopped fiber composite material to the part of the part mold cavity reinforcement NDJ-901-G30 powder (30% chopped glass fiber content, 10.0mm fiber length), mold clamping. After heating in a mold press at 300°C for 1 hour, pressurize it at a pressure of 10 MPa for 10 minutes, and cool to 200°C for demolding. The density of the prepared composite material is 1600kg / m 3 , The tensile strength is 600MPa, and the total molding time is 70 minutes.
Embodiment 3
[0028] Lay the T300 carbon fiber 12K wire flat at 280g / m 2 Spread 1 piece of 0.1mm thermoplastic polyimide film on and under the carbon fiber, fiber / film=50 / 50. For 2mm thick parts, 11 layers can be laid. The film and the carbon fiber and glass fiber braid are layered in turn. Put the layered carbon fiber and thermoplastic polyimide film into the skin part of the mold cavity of the part, and add 40 pieces of thermoplastic polyimide-based chopped fiber composite material NDJ-901-ECG to the reinforcement part of the mold cavity Material (the content of chopped glass fiber and carbon fiber are 15% and 25%, and the fiber length is 1.00mm), and then the mold is closed. After heating for 0.8 hours in a mold press at 360°C, pressurize at a pressure of 25MPa for 7 minutes, and cool to 200°C for demolding. The density of the prepared composite material is 1500kg / m 3 , The tensile strength is 800MPa, and the total molding time is 55 minutes.
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