Bonding type optical film and adhesive composition
An optical film, adhesive type technology, applied in the direction of film/sheet adhesive, adhesive type, ester copolymer adhesive, etc., can solve problems such as poor durability, coloration, and decreased near-infrared absorption capacity , to achieve the effect of reducing the number of layer structures and high pigment durability
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manufacture example 1
[0108]
[0109] Butyl acrylate (412.7 g), methyl acrylate (117.9 g), and acrylic acid (10.4 g) were weighed and mixed well as monomers to obtain a polymerizable monomer mixture (A1). 160 g of ethyl acetate and 300 g of the polymerizable monomer mixture (A1) were charged into the flask. In addition, 300g of the polymerizable monomer mixture (A1), 16g of ethyl acetate and 0.15g of Naipa-BMT-K40 (polymerization initiator, produced by NOF Co., Ltd.) were added to the dropping funnel, and fully mixed to make a solution for dropping. Mixture (A2). While blowing nitrogen gas at 20ml / min, the temperature in the flask was raised to 95°C, and the polymerization initiator Naipa-BMT-K40 (0.15g) was put into the flask to initiate the polymerization reaction. The dropping mixture (A2) was dropped from the dropping funnel over 90 min. After completion of dripping the mixture for dripping (A2), aging was performed for 6 hours while diluting with ethyl acetate according to the increase in ...
manufacture example 2
[0110]
[0111] Butyl acrylate (458.6 g), methyl acrylate (131.0 g), and acrylic acid (10.4 g) were weighed and mixed well as monomers to obtain a polymerizable monomer mixture (B1). 160 g of ethyl acetate and 300 g of the polymerizable monomer mixture (B1) were charged into the flask. In addition, 300g polymerizable monomer mixture (B1), 16g ethyl acetate and 0.15g Naipa-BMT-K40 (polymerization initiator, produced by NOF Co., Ltd.) were added in the dropping funnel, and fully mixed to make the mixture for dropping ( B2). While blowing nitrogen gas at 20ml / min, the temperature inside the flask was raised to 95°C, and the polymerization initiator Naipa-BMT-K40 (0.15g) was put into the flask to initiate the polymerization reaction. The dropping mixture (B2) was dropped from the dropping funnel over 90 min. After completion of dripping the mixture for dripping (B2), aging was performed for 6 hours while diluting with ethyl acetate according to the increase in viscosity, and a...
manufacture example 3
[0112]
[0113] Butyl acrylate (409.1 g), methyl acrylate (116.9 g), and acrylic acid (15.6 g) were weighed and mixed well as monomers to obtain a polymerizable monomer mixture (C1). 160 g of ethyl acetate and 300 g of the polymerizable monomer mixture (C1) were charged into the flask. In addition, 300g of the polymerizable monomer mixture (C1), 16g of ethyl acetate and 0.15g of Naipa-BMT-K40 (polymerization initiator, produced by NOF Co., Ltd.) were added to the dropping funnel, and fully mixed to make a solution for dropping. Mixture (C2). While blowing nitrogen gas at 20 ml / min, the temperature inside the flask was raised to 95° C., and the polymerization initiator Naipa-BMT-K40 (0.15 g) was put into the flask to initiate the polymerization reaction. The dropping mixture (C2) was dropped from the dropping funnel over 90 min. After completion of dripping the mixture for dripping liquid (C2), aging was performed for 6 hours while diluting with ethyl acetate according to t...
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