Preparation methods of welsh onion oil and dietary fibers of welsh onion
A technology of dietary fiber and scallions, applied in food preparation, food science, edible oil/fat, etc., can solve the problems of low deep processing of scallions, achieve good development and utilization prospects, realize comprehensive processing and utilization, and simple and easy process operation Effect
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Embodiment 1
[0025] (1) Wash and homogenize the fresh scallions;
[0026] (2) Take 500g of homogenate, add 1.5 times of water, steam distill at 106°C for 4h, collect volatile oil, anhydrous Na 2 SO 4 Remove residual water to obtain 1.0 g of pure shallot oil.
[0027] The extracted scallion oil is light yellow clear oil with little irritation and fresh scallion flavor, and the yield of scallion oil is 2.0‰. Detected by gas chromatography-mass spectrometry (GC-MS), the content of disulfide compounds in the shallot oil is 35.65%, the content of trisulfides is 23.5%, and the content of thiosulfonate is 7.84%. The specific components are shown in the table 1.
[0028] (3) Add water to the distilled green onion residue, the mass ratio of green onion residue to water is 1:1, extract at 50° C. for 4 hours, and filter to separate the filtrate and filter residue.
[0029] (4) 5 times of volume of 93% ethanol precipitation is added to the filtrate obtained in step (3), the precipitate is adjusted...
Embodiment 2
[0032] (1) Wash and homogenize the fresh scallions first,
[0033] (2) Take 500g of homogenate, add 2 times of water, steam distill at 103°C for 4.5h, collect volatile oil, anhydrous Na 2 SO 4 Remove residual water to obtain 1.1 g of pure shallot oil.
[0034] The extracted scallion oil is light yellow clear oil with little irritation and fresh scallion flavor, and the yield of scallion oil is 2.2‰. Detected by gas chromatography-mass spectrometry (GC-MS), the content of disulfide compounds in the shallot oil is 35.79%, the content of trisulfides is 25.23%, and the content of thiosulfonate is 7.67%. The specific components are shown in the table 1.
[0035] (3) Add water to the distilled green onion residue, the mass ratio of green onion residue to water is 1:2, extract at 55° C. for 5 hours, and filter to separate the filtrate and filter residue.
[0036] (4) 3 times of volume of 93% ethanol precipitation is added to the filtrate obtained in step (3), the precipitate is a...
Embodiment 3
[0039] (1) Wash and homogenize the fresh scallions;
[0040] (2) Take 500g of homogenate, add 2.5 times of water, steam distillation at 109°C for 5.5h, collect volatile oil, anhydrous Na 2 SO 4 Remove residual water to obtain 1.0 g of pure shallot oil.
[0041] The extracted scallion oil is light yellow clear oil with little irritation and fresh scallion flavor, and the yield of scallion oil is 2.0‰. Detected by gas chromatography-mass spectrometry (GC-MS), the content of disulfide compounds in the shallot oil is 33.43%, the content of trisulfides is 24.57%, and the content of thiosulfonate is 7.26%. The specific components are shown in the table 1.
[0042] (3) Add water to the distilled green onion residue, the mass ratio of green onion residue to water is 1:1.5, extract at 60° C. for 4.5 hours, and filter to separate the filtrate and filter residue.
[0043](4) 4 times of volume of 93% ethanol precipitation is added to the filtrate obtained in step (3), the precipitate ...
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