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Device for simultaneously scorching at multiple sections in catalyst device of fixed bed reactor and process thereof

A fixed-bed reactor and catalyst technology, applied in catalyst regeneration/reactivation, physical/chemical process catalysts, chemical instruments and methods, etc. Inactivation and other problems, to achieve the effect of shortening the scorching time, monitoring the oxygen content, and reducing the energy consumption of the device

Active Publication Date: 2013-03-20
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although this invention realizes the coking of multi-stage catalysts at the same time, the coking temperature of the subsequent two stages of the catalyst bed cannot be controlled, and the oxygen content cannot be controlled, which can easily lead to overheating of the catalyst bed, and there is no way to cool down once the overtemperature occurs. measures, the catalyst is easily deactivated by high temperature sintering

Method used

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  • Device for simultaneously scorching at multiple sections in catalyst device of fixed bed reactor and process thereof
  • Device for simultaneously scorching at multiple sections in catalyst device of fixed bed reactor and process thereof
  • Device for simultaneously scorching at multiple sections in catalyst device of fixed bed reactor and process thereof

Examples

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Effect test

Embodiment 1

[0028] The multi-stage simultaneous coking device in the fixed bed multi-bed reactor catalyst includes a heating furnace, a regeneration cycle gas compressor, a catalyst reactor, a regeneration cycle gas liquid separation tank, an online oxygen analyzer and a regulating valve. There are two A catalyst bed is divided into an upper bed 8 and a lower bed 9, and a pipeline C12 communicated with the pipeline A10 is set between the outlet pipeline A10 of the regeneration cycle gas compressor and the inlet of the lower bed 9, and a pipeline C12 connected with the pipeline C12 is arranged on the pipeline C12. Connected make-up compressed air line F15. A regenerative circulating air regulating valve 6 and a compressed air regulating valve A5 are respectively provided at the inlet end of the pipeline C12 and the outlet end of the supplementary compressed air pipeline F15. The online oxygen analyzer is set between the connection between the supplementary compressed air line F15 and the l...

Embodiment 2

[0047] The multi-stage simultaneous coking device in multiple fixed-bed catalyst reactors in series includes a heating furnace, a regeneration cycle gas compressor, a catalyst reactor, a regeneration cycle gas liquid separation tank, an online oxygen analyzer and a regulating valve, reactor A and reactor B In series, there are single beds in the reactor, which are respectively bed 8 and bed 9, and a pipeline C12 connected with pipeline A10 is set between the outlet pipeline A10 of the regeneration cycle gas compressor and the inlet of bed B. C12 is provided with a make-up air pipeline F15 communicating with it. Flow control valves are respectively provided at the inlet end of the pipeline C12 and the outlet end of the supplementary air pipeline F15. The online oxygen analyzer is set between the connection between the air supply line F15 and the line C12 and the inlet of the bed B.

[0048] The coking process and related process parameters, time and consumption of the multi-st...

Embodiment 3

[0050] The fixed-bed multi-bed reactor catalyst regeneration coking device includes a heating furnace, a regeneration cycle gas compressor, a catalyst reactor, a regeneration cycle gas liquid separation tank and a regulating valve.

[0051] The coke regeneration process in the fixed-bed multi-bed reactor catalyst includes the following steps:

[0052] (1) Start the regenerative cycle gas compressor, fill it with nitrogen from its inlet, and increase the pressure to 0.3MPa-0.4MPa;

[0053] (2) The heating furnace is ignited and heated up, and the system is replaced with hot nitrogen, and the temperature is raised to 395-405 °C at the outlet of the heating furnace;

[0054] (3) Open the compressed air regulating valve B7 to replenish compressed air from the inlet of the regenerated circulating air compressor, start to burn from the top of the reactor, and control the oxygen content to be about 0.5%, which is the first stage of burning;

[0055] (4) When the temperature of the c...

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Abstract

The invention relates to a novel regenerative scorching device for a fixed bed catalyst and a process thereof, in particular to a device for simultaneously scorching in a fixed bed multi-bed catalyst reactor and a process thereof as well as a device for simultaneously scorching catalysts in multiple fixed bed reactor series connectors and a process thereof. The technical scheme of the invention is that: a device for simultaneously scorching at multiple sections in a catalyst device of a fixed bed reactor comprises a heating furnace, a regenerative recycle gas compressor, a catalyst reactor and a regenerative recycle gas liquid separation tank, wherein a catalyst bed is formed in the reactor; a pipeline which is communicated with an outlet pipeline of the regenerative recycle gas compressor is arranged between the outlet pipeline and the lower section bed inlets of two adjacent beds; and the pipeline is provided with a compressed air replenishing pipeline which is communicated with the pipeline. Due to the adoption of the device and the process, the scorching time of a catalyst can be shortened, gas, industrial electricity and circulating water can be saved, the energy consumption of the device can be lowered, the scorching safety can be ensured, and the production capability of the device can be increased.

Description

technical field [0001] The present invention relates to a novel regenerative coking device for fixed-bed catalysts and its technology, in particular to the coking device in a fixed-bed multi-bed catalyst reactor and its technology, and the simultaneous coking device for catalysts in multiple fixed-bed reactor series devices and its craft. Background technique [0002] At present, there are two kinds of coking methods commonly used in the industry for regeneration of fixed-bed catalysts: internal regeneration and external regeneration. The present invention only relates to the in-vessel regeneration coke of fixed-bed multi-bed catalysts or the catalyst regeneration coke in multiple fixed-bed reactors in series. In the traditional multi-stage fixed bed catalyst coking, the compressed air is added to the top of the catalyst reactor, and the coking is carried out layer by layer from the top until it penetrates the entire bed, and the coking ends after there is no obvious change...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J38/14B01J38/02
Inventor 郑海张艺峰竺家培钟湘生雷平
Owner CHINA PETROLEUM & CHEM CORP
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