Method for recovering spilled oil in water area
A recovery method and oil spill technology, applied in the separation method, grease/oily substance/suspended matter removal device, liquid separation, etc., can solve the problems of high cost and many processes, achieve good effect, simple implementation materials, and oil spill The effect of high recovery rate
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[0032] The preparation method of the SiFast-332 is as follows:
[0033] Get 5-40 parts of sodium dodecyl perfluorosulfonate, 5-65 parts of polysiloxane compound with the following structural formula,
[0034]
[0035] Then mix it with 10-50 parts of alcohol containing 1-4 carbon atoms and 10-40 parts of water, heat and reflux at 50-70°C, stir evenly for 2-4 hours until the reaction liquid is transparent, and cool to room temperature to prepare.
[0036] The sodium decanyl perfluorosulfonate was purchased from Harbin Xuejia Fluorosilicon Co., Ltd.; the polysiloxane compound was purchased from Qingdao Xingye Organic Silicon New Material Co., Ltd.
[0037] Preferably, 15 parts of sodium dodecyl perfluorosulfonate and 25 parts of the polysiloxane compound shown in the following structural formula,
[0038]
[0039] Then mix it with 30 parts of ethanol and 40 parts of water, heat to reflux at 50°C, and stir evenly for 4 hours until the reaction liquid is transparent, then co...
Embodiment 1
[0044] Take 80g of crude oil, spread it in a circular tank with a diameter of 35cm, and add 4L of seawater. Immerse the oil-absorbing felt of 1.5cm×1.5cm×0.3cm in the oil spill flooding agent SiFast-332 prepared according to the above-mentioned preferred scheme diluted 10 times (the amount of the oil-absorbing felt absorbing the diluted oil spill flooding agent is 0.5g) , take it out, and put it in the center of the above-mentioned round groove covered with oil. The oil surface shrinks rapidly to the edge of the circular groove, and the oil displacement area reaches 95%. The enriched oil was recovered with a peristaltic pump, and the recovery rate reached 92%.
Embodiment 2
[0046] Take 80g of crude oil, spread it in a circular tank with a diameter of 35cm, and add 4L of seawater. The oil-absorbing felt of 1.5cm×1.5cm×0.3cm is immersed in the oil spill flooding agent SiFast-332 prepared according to the above-mentioned preferred scheme diluted 20 times (the amount of oil spill flooding agent absorbed by the oil-absorbing felt is 0.5g) , take it out, and put it in the center of the above-mentioned round groove covered with oil. The oil surface shrinks rapidly to the edge of the circular groove, and the oil displacement area reaches 88%. The enriched oil was recovered with a peristaltic pump, and the recovery rate reached 91%.
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