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Organic fiber cloth filled polymethylmethacrylate composite plate material and its preparation method

A technology of polymethyl methacrylate and methyl methacrylate, applied in the field of composite materials, can solve the problems of poor impact resistance, low hardness, general strength of polymethyl methacrylate, etc. improved effect

Active Publication Date: 2015-06-24
HEFEI GENIUS NEW MATERIALS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The present invention provides a polymethyl methacrylate composite board filled with organic fiber cloth and its preparation method in order to solve the problems of general strength, low hardness and poor impact resistance of polymethyl methacrylate in the prior art.

Method used

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  • Organic fiber cloth filled polymethylmethacrylate composite plate material and its preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] Add 15g of benzoyl peroxide to 1000g of methyl methacrylate and mix evenly, keep warm at 80°C for 10 minutes, vacuum degassing to obtain a prepolymer with moderate viscosity; cut 200g of PA6 fiber cloth and fix it on In the mold, seal the mold. Draw the prepolymer into the mold with negative pressure, feed the material slowly, and keep it warm at 50°C for 10 hours to obtain a semi-finished product after the infiltration is complete; take the semi-finished product out of the mold and put it on a flat vulcanizing machine, and control the pressure at 1MPa to make the PA6 fiber The content of the cloth is kept at about 10%, the temperature is kept at 120° C. for 1 hour, and it is cooled to room temperature to obtain the PA6 fiber cloth-filled polymethyl methacrylate composite sheet.

Embodiment 2

[0021] Add 15g of benzoyl peroxide to 1000g of methyl methacrylate and mix evenly, keep warm at 80°C for 2 minutes, vacuum degassing to obtain a prepolymer with moderate viscosity; cut 300g of PA66 fiber cloth and fix it on In the mold, seal the mold. Draw the prepolymer into the mold by using negative pressure, slowly feed the material, after the infiltration is complete, keep it warm at 50°C for 8 hours to obtain a semi-finished product; take the semi-finished product out of the mold, put it on a flat vulcanizing machine, control the pressure at 5MPa, and make the PA66 fiber cloth The content of polymethyl methacrylate is kept at about 50%, heat preservation at 120°C for 2 hours, and cool to room temperature to obtain PA66 fiber cloth filled polymethyl methacrylate composite board.

Embodiment 3

[0023] Add 15g of benzoyl peroxide to 1000g of methyl methacrylate and mix evenly, keep warm at 80°C for 10 minutes, vacuum degassing to obtain a prepolymer with moderate viscosity; cut 200g of PET fiber cloth and fix it on In the mold, seal the mold. Draw the prepolymer into the mold by using negative pressure, slowly feed the material, after the infiltration is complete, keep it warm at 50°C for 5 hours to obtain a semi-finished product; take the semi-finished product out of the mold, put it on a flat vulcanizing machine, control the pressure at 5MPa, and make the PET fiber cloth The content is kept at about 40%, heat-preserved at 120° C. for 2 hours, and cooled to room temperature to obtain a PET fiber cloth-filled polymethyl methacrylate composite board.

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Abstract

The present invention discloses organic fiber cloth filled polymethylmethacrylate composite plate material and its preparation method. The composite plate material is prepared from methyl methacrylate 40-90 weight parts, organic fiber cloth 10-60 weight parts, and an initiator 0.05-0.2 weight parts. The preparation method comprises adding the initiator into methyl methacrylate to obtain prepolymer, adding the prepolymer into a sealed mold loaded with the organic fiber cloth to obtain a semi-finished product, and pressing, holding at a temperature and cooling on a flat press to obtain the final product. The composite plate material has high strength, excellent impact property and good wear resistance, and greatly widens the application range of polymethylmethacrylate.

Description

technical field [0001] The invention relates to a composite material, in particular to an organic fiber cloth-filled polymethyl methacrylate composite plate and a preparation method thereof. Background technique [0002] Polymethyl methacrylate (PMMA) is a thermoplastic resin, which is the product of bulk polymerization of methacrylic acid. Polymethyl methacrylate is a rigid, hard, colorless and transparent material with a density of 1.18-1.19g / cm3, a tensile strength of 50-77MPa, and a bending strength of 90-130MPa. It has excellent weather resistance, chemical stability and processing performance. However, polymethyl methacrylate has low hardness, poor heat resistance and impact resistance, is easy to crack under stress, and its elongation at break is only 2%-3%. Contents of the invention [0003] The present invention provides an organic fiber cloth-filled polymethyl methacrylate composite board and a preparation method thereof in order to solve the problems of genera...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L33/12C08L77/02C08L77/06C08L67/02B29C70/50
Inventor 李万里
Owner HEFEI GENIUS NEW MATERIALS