Method for testing fluorine ions in fluoride paint
A detection method and fluoride ion technology, applied in the direction of electrochemical variables of materials, etc., can solve the problems of long fluoride ion time, unstable analysis data, large interference, etc., and achieve the effect of rapid analysis
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[0039] 1), electrode positioning correction
[0040] ①First prepare the ionic strength regulator:
[0041] Weigh C 6 H 12 N 4 (Hexamethylenetetramine)142g, KNO 3 (Potassium nitrate) 85g, C 6 H 4 Na 2 O 8 S 2 ·H 2 O (1,2-dihydroxybenzene-3,5-disulfonate sodium titanium iron reagent) 9.97g, dissolved in a 1000ML volumetric flask, diluted with water to the mark, and mixed well.
[0042] ② Put 30ml of 10ppm fluoride ion stock solution and 30ml of ionic strength regulator (TISAB) into a 100ml plastic beaker, mix thoroughly, immerse the electrode in the mixed solution, and correct the electrode position.
[0043] 2) Slope correction of fluoride ion detector
[0044] Put 30ml of 1ppm fluoride ion stock solution and 30ml of ionic strength regulator into a 100ml plastic beaker, and after thoroughly mixing, immerse the electrode in the mixed solution to correct the slope of the electrode.
[0045] 3), measurement steps
[0046] (1) Calibration of ion concentration meter
[0047] ① After cleaning the...
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