Traditional Chinese medicine composition with anticancer effect and preparation method and detection method thereof
A composition and technology of traditional Chinese medicine, applied in the field of traditional Chinese medicine, can solve the problems of large trauma, unsatisfactory curative effect and high risk for patients
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Embodiment 1
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[0174]
[0175] The above thirty-four medicinal herbs, turtle shells, decoct 3 times (add 9 times the water), 3 hours each time, combine the decoction, filter, and concentrate the filtrate to an appropriate amount (about 180ml); Angelica, Chuanxiong, Turmeric, Galangal , cinnamon, clove, asafoetida, and balsamic extract by steam distillation for 6 hours (add 12 times of water), collect volatile oil and distillate (about 50ml), decoct the dregs and other twenty-five flavors with water three times, the first time 2 hours (add 12 times of water), 1.5 hours each for the second and third times (add 10 times and 8 times of water respectively), combine the decoction, filter, and concentrate the filtrate to a clear paste with a relative density of 1.15 (50-60°C), add ethanol Make the alcohol content reach 70%, adjust the pH value to 7.5-8.0, let it stand (0-5°C) for 24 hours, filter, recover ethanol from the filtrate, add water to a clear paste with a relative density of...
Embodiment 2
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[0179] The above thirty-four flavors, turtle shells were decocted with 9 times the amount of water for 3 times, each time for 3 hours, combined the decoction, filtered, and the filtrate was concentrated to 180ml; angelica, chuanxiong, turmeric, galangal, cinnamon, cloves, ferulae Add 12 times the amount of water for Jiangxiang and extract for 6 hours. Collect about 50ml of volatile oil and aromatic water. Add 10 times the amount of water, decoct for 1.5 hours, combine the decoction, concentrate to a relative density of about 1.15, add ethanol to make the alcohol content reach 70%, adjust the pH value to 7.5-8.0, let stand for 24 hours, filter, and recover the filtrate Ethanol, add water to a relative density of about 1.06, then add turtle shell decoction, boil for 20 minutes, let cool, add volatile oil, aromatic water, Tween-802‰, cyclamate 2‰, add water to 1000ml, let stand for 24-48 hours , take the supernatant, potting, sterilizing, packaging, to get...
Embodiment 3
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[0182] Preparation method: the above thirty-four flavors, boil the turtle shell with water for 3 times, each time for 3 hours, combine the decoction, filter, and concentrate the filtrate to an appropriate amount; Steam distillation and extraction of balsamic perfume for 6 hours, collect volatile oil and appropriate amount of distillate, decoct medicinal residues and other twenty-five flavors with water three times, 2 hours for the first time, 1.5 hours for the second and third times, combine the decoction, filter, and filtrate Concentrate to a clear paste with a relative density of about 1.15 (50-60°C), add ethanol to make the alcohol content reach 70%, adjust the pH value to 7.5-8.0, let it stand for 24 hours, filter, recover ethanol from the filtrate, add water to the relative density About 1.06 (50 ~ 60 ℃) clear ointment, then add turtle shell decoction, boil for 20 minutes, let cool, add volatile oil and distillate, and make granules by conventional technology. ...
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