Polydicyclopentadiene building template material and its preparation method
A technology of polydicyclopentadiene and dicyclopentadiene, which is applied in the field of preparation of the material, can solve problems such as application limitations, manufacturing difficulties, poor stiffness, etc., achieve multiple times of repeated use, improve impact strength, and overcome easy water absorption Effect
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Embodiment 1
[0031] The polydicyclopentadiene building template material of this embodiment is obtained by blending and polymerizing the following raw materials in weight percentage: 98.5% polydicyclopentadiene and 1.5% glass fiber, and the length of the glass fiber is 10 mm.
[0032] The preparation method of polydicyclopentadiene building template material of the present invention comprises the following steps:
[0033] (1) Under the condition of 45°C, 1.5% by weight glass fibers are uniformly dispersed in 98.5% by weight dicyclopentadiene through a homogenizer to obtain a dicyclopentadiene mixed solution in which glass fibers are uniformly dispersed , the vacuum pump is degassed for 25 minutes and then filled with nitrogen for protection;
[0034] (2) under nitrogen protection, add 25 kilograms of dicyclopentadiene mixed liquids in which glass fibers are evenly dispersed in tank A and tank B of the reaction injection molding machine respectively; then add 0.261 kilograms of di(2,6 di t...
Embodiment 2
[0038] The polydicyclopentadiene building formwork material of this embodiment is obtained by blending and polymerizing the following raw materials in weight percentage: 99.7% dicyclopentadiene and 0.3% glass fiber, and the length of the glass fiber is 1 mm.
[0039] The preparation method of polydicyclopentadiene building template material of the present invention comprises the following steps:
[0040] (1) Under the condition of 45°C, 0.3% by weight glass fibers are uniformly dispersed in 99.7% by weight dicyclopentadiene through a homogenizer to obtain a dicyclopentadiene mixed solution in which glass fibers are uniformly dispersed , the vacuum pump is degassed for 25 minutes and then filled with nitrogen for protection;
[0041] (2) Add respectively 25 kilograms of dicyclopentadiene mixed solutions in which glass fibers are uniformly dispersed in tank A and tank B of the reaction injection molding machine under nitrogen protection; then add 0.138 kilograms of bis(2,6 Dite...
Embodiment 3
[0045] The polydicyclopentadiene building formwork material of this embodiment is composed of the following components by weight percentage: 99% polydicyclopentadiene and 1% surface coupling modified glass fiber, wherein the length of the glass fiber is 3mm.
[0046] The preparation method of polydicyclopentadiene building template material of the present invention comprises the following steps:
[0047](1) Add 1 gram of glass fiber to 75 grams of KH-570 silane coupling agent acetone solution with a mass fraction of 10%, add glacial acetic acid to adjust the pH value to 4.5, then disperse and react with ultrasonic waves for 5 hours, and control the water temperature at 60°C After the reaction, the surface-coupling modified glass fiber is taken out, washed with distilled water until the pH is 7, and dried in a vacuum oven at 80°C to constant weight to obtain the surface-coupling modified glass fiber;
[0048] (2) Under the condition of 45°C, uniformly disperse the surface coupl...
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