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Method for reducing error in polar altitude vacuum measurement of ESD (Electro Simulated Desorption) neutral particles

An electronic excitation, neutral particle technology, applied in the field of measurement, can solve problems such as indistinguishability, and achieve the effect of extending the lower limit of accurate measurement and reducing errors

Active Publication Date: 2013-02-13
NO 510 INST THE FIFTH RES INST OFCHINA AEROSPAE SCI & TECH
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Problems solved by technology

[0004] The purpose of the present invention is to provide a very high vacuum measurement method that reduces the error of electronically excited desorption neutral particles. The method solves the problem that the separation gauge in the full pressure measurement can effectively separate ESD ions and gas phase ions, but cannot distinguish gas phase ions. The problem of ion generation from doped ESD neutral particles; reduces the error of extremely high vacuum measurement and extends the lower limit of accurate measurement

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  • Method for reducing error in polar altitude vacuum measurement of ESD (Electro Simulated Desorption) neutral particles

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Embodiment 1

[0028] A very high vacuum measurement method for reducing the error of electron-excited desorption neutral particles, the device used in the method includes: a vacuum valve 1, an ionization gauge 2, a vacuum chamber 3, a vacuum pump group 4 and a quadrupole mass spectrometer 5; wherein, The vacuum valve 1, the ionization gauge 2, the vacuum pump group 4, and the quadrupole mass spectrometer 5 are respectively connected with the vacuum chamber 3, such as figure 1 shown;

[0029] The quadrupole mass spectrometer 5 is a quadrupole mass spectrometer 5 that is equipped with an energy analyzer between the ion source and the quadrupole rod to separate electron-excited desorption ions and gas-phase ions;

[0030] The vacuum valve 1 is an all-metal structure;

[0031] The measurement lower limit of described ionization gauge 2 is 10 -10 Pa level;

[0032] The method steps are as follows:

[0033] (1) Keep the vacuum valve 1 closed, turn on the vacuum pump group 4, and pump air to t...

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Abstract

The invention discloses a method for reducing error in polar altitude vacuum measurement of ESD (Electro Simulated Desorption) neutral particles, and belongs to the field of measurement. Devices adopted in the method include a vacuum valve, an ionization gauge, a vacuum chamber, a vacuum pump group and a quadrupole mass spectrograph, wherein the vacuum valve, the ionization gauge, the vacuum pump group and the quadrupole mass spectrograph are respectively connected with the vacuum chamber; the quadrupole mass spectrograph is capable of separating electron excitation desorption ions and gas-phase ions and an energy analyzer is installed between an ion source and a quadrupole rod; the vacuum valve is of a full metal structure; and the lower measurement limit of the ionization gauge is 10-10Pa magnitude. By utilizing the method, the problem that in the full-pressure measurement, the ionization gauge and the like can effectively separate ESD ions and gas phase ions but cannot discriminate ions generated from ESD neutral particles doped in the gas phase ions is solved; the error in polar altitude vacuum measurement is reduced; and the lower limit in accurate measurement is extended.

Description

technical field [0001] The invention relates to an extremely high vacuum measurement method for reducing the error of electron stimulated desorption (ESD) neutral particles, especially the ultrahigh / extremely high vacuum system realized by adopting a quadrupole mass spectrometer with an energy analyzer structure The invention relates to a method for measuring vacuum degree, which belongs to the field of measurement. Background technique [0002] The ESD effect on the grid surface of the hot cathode ionization gauge will generate ESD ions and ESD neutral particles, and the ESD ions and gas phase ions have an energy difference. The document "Development of Extremely High Vacuum Technology, "Aerospace Measuring Technology" Volume 29, Issue 5, 2009, Page 71-76", introduces a variety of effective separation of ESD ions, reducing the limiting factors of extremely high vacuum measurement That is, the extremely high vacuum ionization gauge of ESD effect. The literature pointed out...

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01L21/30
Inventor 习振华李得天冯焱成永军马奔刘珈彤
Owner NO 510 INST THE FIFTH RES INST OFCHINA AEROSPAE SCI & TECH
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