A method for extracting polysaccharides from buckwheat bran
A technology of buckwheat bran and polysaccharides, which is applied in the production process of buckwheat polysaccharides and can solve problems such as side effects
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Embodiment 1
[0008] Weigh 100 kg of buckwheat bran, add 5 times the amount of water respectively, extract 3 times at 70 ° C for 2 h, combine the extracts, centrifuge to remove insolubles, and put the filtrate on a macroporous adsorption resin AB-8 column (10 × 150 cm). Elute with ionized water, then elute with 5% and 10% ethanol respectively, combine and concentrate the eluents, add 4 times of 95% ethanol while stirring, let stand for 12 hours, and obtain white crude polysaccharide precipitate after centrifugation , vacuum-dried the precipitate to obtain buckwheat polysaccharide.
Embodiment 2
[0010] Weigh 100 kg of buckwheat bran, add 15 times the amount of water respectively, extract 3 hours at 60 ° C for 3 hours, combine the extracts, centrifuge to remove insolubles, and put the filtrate on a macroporous adsorption resin AB-8 column (10 × 150 cm). Elute with ionized water, then elute with 5% and 10% ethanol respectively, combine and concentrate the eluents, add 4 times of 95% ethanol while stirring, let stand for 12 hours, and obtain white crude polysaccharide precipitate after centrifugation , vacuum-dried the precipitate to obtain buckwheat polysaccharide.
Embodiment 3
[0012] Weigh 100 kg of buckwheat bran, add 20 times the amount of water respectively, extract 4 hours at 80 ° C, extract 3 times, combine the extracts, centrifuge to remove insolubles, and put the filtrate on a macroporous adsorption resin AB-8 column (10 × 150 cm). Elute with ionized water, then elute with 5% and 10% ethanol respectively, combine and concentrate the eluents, add 4 times of 95% ethanol while stirring, let stand for 12 hours, and obtain white crude polysaccharide precipitate after centrifugation , vacuum-dried the precipitate to obtain buckwheat polysaccharide.
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