Modified composite titanium-based grease of micron-nano particles and preparation method thereof

A technology of micro-nano particles and composite titanium, applied in the direction of lubricating composition, etc., can solve the problem of low friction and anti-wear performance of composite titanium-based grease, and achieve the effects of good self-healing performance, reduced friction coefficient and broad market prospects.

Inactive Publication Date: 2013-05-22
尹继辉 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] In order to solve the problem that the anti-friction and anti-wear performance of the existing composite titanium-based greas

Method used

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  • Modified composite titanium-based grease of micron-nano particles and preparation method thereof

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specific Embodiment approach 1

[0012] Specific embodiment 1: The micro-nano particle modified composite titanium-based lubricating grease of this embodiment is composed of 70-90 parts by mass of base oil, 2-9 parts of fatty acid, and 4-18 parts of tetraisopropyl titanate ester, 1-4 parts of aromatic acid, 0.5-1.5 parts of diphenylamine, 2-4 parts of magnesium hydroxysilicate powder and 1-2 parts of nano-grease additive; wherein the particle size of magnesium hydroxysilicate powder is 1~5μm.

[0013] The micro-nano particle modified composite titanium-based grease of this embodiment makes the prepared composite titanium-based grease have good self-healing properties by adding micro-nano-level additives such as hydroxymagnesium silicate powder and nano-rare earth compounds with self-repairing properties. performance.

specific Embodiment approach 2

[0014] Specific embodiment two: The difference between this embodiment and specific embodiment one is that the micro-nano particle modified composite titanium-based lubricating grease is composed of 75-85 parts by mass of base oil, 4-8 parts of fatty acid, 8-8 parts 16 parts of tetraisopropyl titanate, 2 to 3 parts of aromatic acid, 0.8 to 1.3 parts of diphenylamine, 2.5 to 3.5 parts of magnesium hydroxysilicate powder and 1.2 to 1.8 parts of nano lubricating oil additive; wherein hydroxyl The particle size of the magnesium silicate powder is 1-5 μm, and other steps and parameters are the same as those in Embodiment 1.

specific Embodiment approach 3

[0015] Specific embodiment three: the difference between this embodiment and specific embodiment one or two is: the base oil is one or more mixtures in any ratio of mineral oil, synthetic oil or vegetable oil, other steps and parameters are the same as The specific embodiment 1 or 2 are the same.

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Abstract

The invention relates to modified composite titanium-based grease of micron-nano particles and a preparation method thereof. In order to solve the problem of low antiwear and friction reduction properties of existing composite titanium-based grease, the preparation method comprises the following steps of firstly, mixing fatty acid and a part of base oil and then adding tetraisopropyl titanate, aromatic acid and distilled water; pre-heating the residual base oil and then adding the residual base oil to a reaction system, adding diphenylamine and a micron-nano additive, and grinding after the reaction is finished to obtain the modified composite titanium-based grease of the micron-nano particles. Compared with the composite titanium-based grease, the friction coefficient is reduced by 16.9-29.3%; the diameter of a wear spot is reduced by 21.4-32.7%; the antiwear and friction reduction properties are improved; the prepared composite titanium-based grease has good self-repairing performance by adding hydroxyl magnesium silicate powder with the self-repairing performance; and the modified composite titanium-based grease can be applied to various mechanized equipments and devices.

Description

technical field [0001] The invention relates to a lubricating grease modified by micronano particles and a preparation method thereof. Background technique [0002] Friction and wear is a ubiquitous phenomenon in nature. According to statistics, friction consumes 1 / 3 to 1 / 2 of the world's energy, and wear is one of the main forms of failure and destruction of equipment and materials. About 80% of parts are damaged due to Wear and tear, and the use of lubricating grease can effectively reduce friction and wear. Although the output of lubricating grease only accounts for about 5% of lubricating oil output, it is widely used in rolling, rotating, sliding and other parts that cannot be lubricated by lubricating oil, such as bearings and gears, and occupies a very important position in the national economy. As heavy load, high speed, high temperature and other equipment are more and more widely used in modern industry, various departments of industrial production have put forwar...

Claims

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Application Information

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IPC IPC(8): C10M169/06
Inventor 尹继辉郁向民
Owner 尹继辉
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