Organic green material [(2,4,6-trimethylphenyl)-pyridine-2-methyleneamine]HgCl2 and synthetic method thereof
A technology of trimethylphenyl and methylene amine, which is applied in the field of organic green light materials and their synthesis, can solve problems such as complex synthesis methods, and achieve the effects of simple and easy operation, high yield and strong stability
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
specific Embodiment approach 1
[0015] Specific implementation mode 1: The organic green light material [(2,4,6-trimethylphenyl)-pyridine-2-methyleneamine]HgCl in this implementation mode 2 The molecular formula is C 15 h 16 Cl 2 N 2 Hg, whose structural formula is
[0016]
specific Embodiment approach 2
[0017] Embodiment 2: The organic green light material [(2,4,6-trimethylphenyl)-pyridine-2-methyleneamine]HgCl of Embodiment 1 2 The synthetic method is characterized in that the organic green light material [(2,4,6-trimethylphenyl)-pyridine-2-methyleneamine] HgCl 2 The synthetic method of carries out according to the following steps:
[0018] 1. Mix 20~25mg (2,4,6-trimethylphenyl)-pyridine-2-methyleneamine and 25~30mg anhydrous HgCl 2 Dissolve in a mixed organic solvent, heat to reflux, and stir for 5 hours to obtain a yellow reaction liquid;
[0019] 2. Filter the product of step 1 while it is hot, and then volatilize at room temperature for 3 to 10 days to obtain [(2,4,6-trimethylphenyl)-pyridine-2-methyleneamine]HgCl 2 ; The mixed organic solvent described in step one is CH 3 OH and CH 2 Cl 2 mixed solution of CH 3 OH and CH 2 Cl 2 The volume ratio is 1:5.
[0020] The productive rate of this embodiment is 65.20%. [(2,4,6-trimethylphenyl)-pyridine-2-methyleneamine]...
specific Embodiment approach 3
[0023] Specific embodiment three: this embodiment is the same as specific embodiment two in that in step one, 21 to 24 mg (2,4,6-trimethylphenyl)-pyridine-2-methyleneamine and 26 to 29 mg of water HgCl 2 Soluble in mixed organic solvents. Others are the same as in the second embodiment.
PUM
Property | Measurement | Unit |
---|---|---|
emission peak | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com