High-temperature annular protection sealing liquid for water injection well

An annular protection and sealing fluid technology, applied in the field of oilfield water injection well annular protection and amide high temperature rings, can solve the problems of using special equipment and poor effect, and achieve the effects of low pumping resistance, improved validity period and long validity period

Active Publication Date: 2013-09-11
中国石油化工股份有限公司华东油气分公司泰州采油厂
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Aiming at the problem of limited use of packers, many oilfields in China have carried out research on replacing packers with chemical gels and made great progress. However, in the actual production process, the existing technologies still have many shortcomings and limitations, such as If the well depth is more than 1500m, the effect is poor, and the operating temperature is lower than 60°C. It is necessary to prepare liquid 1-3 days in advance, and special equipment is required for liquid preparation on the ground.

Method used

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  • High-temperature annular protection sealing liquid for water injection well

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0052] Pour 3.5Kg of acrylamide into a water tank filled with 95.693Kg of water, and at the same time, the pump truck circulates and stirs; while circulating and stirring, add 0.5Kg of formaldehyde, 0.3Kg of phenol, 0.006Kg of azobisisobutylcyanide, and 0.001Kg of ferricyanide in sequence Potassium chloride is used to obtain the base fluid 1 of the annulus protection sealing fluid.

Embodiment 2

[0054] Pour 5.0Kg of acrylamide into a water tank filled with 93.29Kg of water, and at the same time, the pump truck circulates and stirs; while circulating and stirring, add 1.0Kg of formaldehyde, 0.70Kg of phenol, 0.008Kg of azobisisobutylcyanide, and 0.002Kg of ferricyanide in sequence Potassium chloride is used to obtain the base fluid 2 of the annulus protection sealing fluid.

Embodiment 3

[0056] Pour 6.0Kg of acrylamide into a water tank filled with 91.485Kg of water, and at the same time, the pump truck circulates and stirs; while circulating and stirring, add 2.0Kg of formaldehyde, 0.50Kg of phenol, 0.01Kg of azobisisobutylcyanide, and 0.005Kg of ferricyanide in sequence Potassium chloride is used to obtain the base fluid 3 of the annulus protection sealing fluid.

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Abstract

The invention discloses a high-temperature annular protection sealing liquid for a water injection well. A base fluid is prepared from the following compositions in percentage by weight: 3.5-10% of gelatinizing agent, 0.5-3% of crosslinking agent A, 0.3-1.0% of crosslinking agent B, 0.006-0.015% of initiator, 0.001-0.006% of modifier, and the balance of water, wherein the gelatinizing agent is acrylamide, the crosslinking agent A is formaldehyde, the crosslinking agent B is phenol, the initiator is azodiisobutyronitrile, and the modifier is potassium ferricyanide. The sealing liquid is prepared by the step of crosslinking the base fluid at 70-90DEG C for 4-8 hours or at 100-130DEG C for 1.5-3 hours. According to the high-temperature annular protection sealing liquid for the water injection well, the manufacture and usage cost is low, the construction is safe and reliable, the annular protection effect for the water injection well is obvious, and the oilfield exploitation production cost can be greatly lowered.

Description

technical field [0001] The invention relates to an annulus protection technology for oilfield water injection wells, in particular to an amide high-temperature annulus [0002] The air protection sealing fluid specifically relates to a high-temperature annular space protection sealing fluid for water injection wells, which is mainly used in water injection wells. Background technique [0003] During the water injection process in the oil field, due to the long-term injection of unqualified water quality, the near-wellbore area, especially the annular space of the oil casing, can easily cause serious deterioration of the water quality, causing a large number of SRB bacteria, iron bacteria and saprophytic bacteria to multiply, resulting in serious damage to the casing. Corrosion, various products increase sharply, causing damage to oil and gas layers, and reducing the service life of water wells. Since the value of a well is several million yuan, in order to prevent the well...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/40
Inventor 陈浩杨怀成程旺林周维斌蒋永平张文正
Owner 中国石油化工股份有限公司华东油气分公司泰州采油厂
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