Preparation method of modified phenolic resin-base friction material
A technology of phenolic resin and friction material, applied in chemical instruments and methods, other chemical processes, etc., can solve the problems of heat resistance, poor toughness, brittleness of phenolic resin, etc., and achieve heat resistance and toughness improvement, heat fading Improved effect
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[0026] Example 1:
[0027] Modified phenolic resin composition: the molar ratio of phenol and formaldehyde is 1.5:1.0, and the mass of bismaleimide is 0.7 times the total mass of phenol and formaldehyde.
[0028] The preparation method of the above modified phenolic resin includes the following steps:
[0029] (1) Weigh the raw material components according to the composition ratio, put phenol and formaldehyde into the reaction kettle, stir and mix the two, and heat to 80°C.
[0030] (2) Add the catalyst, keep stirring, and keep the temperature for 5 hours.
[0031] (3) Add the prescribed amount of bismaleimide to the product obtained in step (2), and stir and mix while adding.
[0032] (4) Adjust the temperature to 80°C, keep it warm and react for 2 hours.
[0033] (5) Heat to 130°C for dehydration for 0.5 hours, cool down to below 50°C, and get ready.
[0034] The weight parts of the modified phenolic resin-based friction material composition are: 20 parts of the above modified phenolic ...
Example Embodiment
[0041] Example 2:
[0042] Modified phenolic resin composition: the molar ratio of cresol and butyraldehyde is 1.2:1.0, and the mass of bismaleimide is 0.5 times the total mass of cresol and butyraldehyde.
[0043] The preparation method of the above modified phenolic resin includes the following steps:
[0044] (1) Weigh the raw material components according to the formula, put the cresol and butyraldehyde into the reaction kettle, stir and mix the two, and then heat to 70°C.
[0045] (2) Add the catalyst, keep stirring, keep the temperature and react for 3 hours.
[0046] (3) Add the prescribed amount of bismaleimide to the product obtained in step (2), and stir and mix while adding.
[0047] (4) Adjust the temperature to 80°C, keep it warm and react for 3 hours.
[0048] (5) Heat to 140°C for dehydration for 1 hour, and cool down to below 50°C to obtain.
[0049] The weight parts of the modified phenolic resin-based friction material are: 15 parts of the above-mentioned modified phenoli...
Example Embodiment
[0056] Example 3:
[0057] Modified phenolic resin composition: the molar ratio of bisphenol and acrolein is 1.7:1.0, and the mass of bismaleimide is 1 time of the total mass of bisphenol and acrolein.
[0058] The preparation method of the above modified phenolic resin includes the following steps:
[0059] (1) Weigh the raw material components according to the composition ratio, put the bisphenol and acrolein into the reactor, stir and mix the two, and then heat to 100°C.
[0060] (2) Add the catalyst, keep stirring, keep the temperature and react for 7 hours.
[0061] (3) Add the prescribed amount of bismaleimide to the product obtained in step (2), and stir and mix while adding.
[0062] (4) Adjust the temperature to 80°C, keep it warm and react for 2 hours.
[0063] (5) Heat to 130°C for dehydration for 0.8 hours, and cool down to below 50°C to obtain.
[0064] The weight parts of the modified phenolic resin-based friction material are: 25 parts of the above modified phenolic resin, 3...
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