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Adhesive and preparation method thereof

A technology of adhesives and curing agents, applied in the direction of modified epoxy resin adhesives, non-polymer adhesive additives, adhesive additives, etc., can solve problems such as easy softening

Inactive Publication Date: 2013-11-20
成都市鑫鸿宇石材有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, in the related art, since the main component of the adhesive is resin, the adhesive is very prone to softening under the condition of 60°C or higher during the bonding process.

Method used

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  • Adhesive and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0012] An adhesive is provided in an embodiment of the present invention, comprising the following components in parts by weight, 2-6 parts of unsaturated resin, 6-10 parts of calcium powder, 0.0006-0.001 part of cobalt water, and 0.0006-0.001 part of curing agent part and 0.1-0.4 part of styrene, more preferably, including 4 parts of unsaturated resin, 8 parts of calcium powder, 0.00084 part of cobalt water, 0.000912 part of curing agent and 0.2 part of styrene.

[0013] Concrete, the choice of unsaturated resin can be various, as unsaturated resin can be 168 resin, 399 resin or 6688 resin, above-mentioned resin all is unsaturated resin, after it is mixed with curing agent and accelerator, It is easier to achieve curing, and the bonding effect is good, especially suitable for bonding glass products. In addition, white water is the preferred curing agent. Because white water has low price and good performance, it is easy to mix with resin and is extremely convenient to use.

...

Embodiment 2

[0019] This embodiment provides a preparation method corresponding to the adhesive provided in the above embodiments, which specifically includes the following steps:

[0020] Step 101: adding cobalt water into the unsaturated resin and stirring to obtain a first solution;

[0021] In step 101, after the cobalt water is added to the unsaturated resin, the first solution is obtained. Specifically, in order to make the cobalt water mix uniformly during the process of adding the unsaturated resin, preferably, the cobalt water is added to the unsaturated resin. During the process, the unsaturated resin is stirred and mixed at the same time, so that the effect of mixing can be achieved.

[0022] Step 102: adding calcium powder into the first solution and stirring to obtain a second solution;

[0023] After obtaining the first solution, it is necessary to add the calcium powder to the first solution. Preferably, in order to make the calcium powder mix with the first solution at a f...

Embodiment 3

[0036] Add 8ml of cobalt water (about 8.4g) to 40kg of 168 unsaturated resin and stir to obtain the first solution; at a temperature of 20°C-28°C, add 80kg of calcium powder to the first solution, and stirred to obtain the second solution; 2 kg of styrene was added to the second solution to obtain the third solution; 8 ml (about 9.12 g) of curing agent was added at a temperature of 20°C-28°C After entering the third solution, stir for 25 minutes to 30 minutes and add to the third solution to obtain an adhesive.

[0037] The adhesive prepared through the steps of Example 3 is experimentally determined to be less likely to soften under the use condition of 60°C.

[0038] In addition, for the adhesive prepared by the preparation method of the above example, since the ratio of the components of the adhesive is optimized, the adhesive is applied to the bonding process, and the bonded board has High toughness, not easy to peel off, crack resistance, corrosion resistance and stampin...

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Abstract

The invention relates to an adhesive and a preparation method thereof. The adhesive is formed by the following components in parts by weight: 2-6 parts of an unsaturated resin, 6-10 parts of calcium powder, 0.0006-0.001 part of cobalt water, 0.0006-0.001 part of a curing agent, 0.1-0.4 part of styrene. The preparation method comprises the following steps: adding cobalt water into the unsaturated resin, stirring to obtain a first solution; adding calcium powder into the first solution, stirring to obtain a second solution; adding styrene into the second solution, stirring to obtain a third solution; adding the curing agent into the third solution, stirring to obtain the adhesive. The adhesive has good heat resistance, and is not easy to soften even at 60 DEG C. Additionally, the calcium powder in the adhesive provided by the invention has anti-aging effect, and the adhesive is not easy to aged even at a lower temperature.

Description

technical field [0001] The invention relates to the field of chemical industry, in particular to an adhesive and a preparation method thereof. Background technique [0002] Adhesives are widely used in aerospace, automotive machinery, construction, chemical industry, light industry, and daily life; common adhesives are mainly composed of resin and curing agent. [0003] However, in the related art, since the main component of the adhesive is resin, the adhesive is very prone to softening under the condition of 60° C. or higher during the bonding process. Contents of the invention [0004] The object of the present invention is to provide an adhesive to solve the above problems. [0005] An adhesive is provided in an embodiment of the present invention, which consists of the following components in parts by weight: 2-6 parts of unsaturated resin, 6-10 parts of calcium powder, 0.0006-0.001 part of cobalt water, and 0.0006-0.001 part of curing agent. 0.001 parts and styrene...

Claims

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Application Information

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IPC IPC(8): C09J163/10C09J11/04
Inventor 曹型语
Owner 成都市鑫鸿宇石材有限公司