Method for detecting elements in alloy
A detection method and element technology, applied in the field of physical and chemical detection, can solve the problems of difficult implementation and long analysis process time.
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Embodiment 1
[0018] 1. A method for detecting Sn element in aluminum alloy. The requirement of Sn element is less than 0.1%. Direct reading spectrometer is used to measure the light intensity ratio to detect the content of impurity elements. The light intensity ratio = (element light intensity / matrix light intensity ) ×100000, including the following steps:
[0019] A. According to the content value of the element to be tested in the aluminum alloy, select the standard sample of Sn element content as 0.095%;
[0020] B. Select and confirm the analysis matrix;
[0021] C. Input the content of the standard sample into the spectrometer, set the excitation parameters, collect the calculated data, excite the standard sample, and obtain the standard light intensity ratio;
[0022] D. Excite the sample to be sent to obtain the light intensity ratio of the sample;
[0023] E. Compare the light intensity ratio of the standard sample and the submitted sample to get the test result.
[0024] If the light int...
Embodiment 2
[0027] 1. A method for detecting Cr element in Fe alloy. Cr element requirement is less than 0.2%. X fluorescence spectrometer is used to measure the light intensity ratio to detect the content of impurity elements. The light intensity ratio = (element light intensity / matrix light intensity )×80000, including the following steps:
[0028] A. According to the content value of the element to be tested in the Fe alloy, select the standard sample with the content of Cr element as 0.2%;
[0029] B. Select and confirm the analysis matrix;
[0030] C. Input the content of the standard sample into the spectrometer, set the excitation parameters, collect the calculated data, excite the standard sample, and obtain the standard light intensity ratio;
[0031] D. Excite the sample to be sent to obtain the light intensity ratio of the sample;
[0032] E. Compare the light intensity ratio of the standard sample and the submitted sample to get the test result.
[0033] If the light intensity ratio o...
Embodiment 3
[0035] 1. A method for detecting Al element in Ti alloy. The requirement of Al element is greater than 0.4%. The light intensity ratio is measured by plasma emission spectrometer to detect the content of impurity elements. The light intensity ratio = (element light intensity / matrix light Strong) × 50000, including the following steps:
[0036] A. According to the content value of the element to be tested in the Ti alloy, select a standard sample with an Al element content of 0.4%;
[0037] B. Select and confirm the analysis matrix;
[0038] C. Input the content of the standard sample into the spectrometer, set the excitation parameters, collect the calculated data, excite the standard sample, and obtain the standard light intensity ratio;
[0039] D. Excite the sample to be sent to obtain the light intensity ratio of the sample;
[0040] E. Compare the light intensity ratio of the standard sample and the submitted sample to get the test result.
[0041] If the light intensity ratio of t...
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