Method for extraction dephenolization of high-concentration chemical wastewater containing phenol ammonia coals
A coal chemical wastewater, high-concentration technology, applied in chemical instruments and methods, extraction water/sewage treatment, water pollutants, etc., can solve the problems of low extraction rate and excessive phenol content, and achieve high extraction rate, cost saving, Guarantee the effect of up-to-standard discharge
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Embodiment 1
[0045] A set of extraction and dephenolization equipment with a treatment capacity of 80 t / h for high-concentration phenol ammonia-containing coal chemical wastewater, with a total phenol content of 5000 mg / L and a COD of 40000 mg / L.
[0046] Using the method for extraction and dephenolation of high-concentration phenolic ammonia-containing coal chemical wastewater of the present invention, butyl acetate and high-concentration phenolic ammonia-containing coal chemical wastewater are pumped into the top and bottom of the extraction tower at a volume ratio of 1:10, and contacted in countercurrent , the extraction temperature is 25°C, the extraction pH is 3.0, and the extraction stage is 1 stage to obtain the extract phase and the raffinate phase;
[0047] Then in the rectification tower, the extraction phase is processed by rectification. The number of rectification towers is 8, the reflux ratio is 0.3, the operating pressure is 0.01 MPa, the operating temperature at the top of t...
Embodiment 2
[0052] A set of extraction and dephenolization equipment with a treatment capacity of 130 t / h of high-concentration phenol ammonia-containing coal chemical wastewater, with a total phenol content of 16320 mg / L, pH=6.0, and COD 32500 mg / L.
[0053] Using the method for extraction and dephenolation of high-concentration phenol ammonia-containing coal chemical wastewater of the present invention, butyl acetate and high-concentration phenol ammonia-containing coal chemical wastewater are pumped from the top and bottom of the extraction tower at a volume ratio of 1:15, and contacted in countercurrent , the extraction temperature is 35°C, the extraction pH=4.0, and the number of extraction stages is 5, to obtain the extract phase and the raffinate phase;
[0054] The extraction phase is rectified, the number of rectification towers is 15, the reflux ratio is 0.4, the operating pressure is 0.04 MPa, the operating temperature at the top of the rectifying tower is controlled at 60°C, an...
Embodiment 3
[0059] A set of extraction and dephenolization equipment with a treatment capacity of 200 t / h for high-concentration phenol ammonia-containing coal chemical wastewater has a total phenol content of 12,800 mg / L, pH=8.7, and COD 37,000 mg / L.
[0060] Using the method for extracting and dephenolizing high-concentration phenolic ammonia-containing coal chemical wastewater of the present invention, butyl acetate and high-concentration phenolic ammonia-containing coal chemical wastewater are pumped into the top and bottom of the extraction tower at a volume ratio of 1:25, and contacted in countercurrent , the extraction temperature is 65°C, the extraction pH=6.0, and the number of extraction stages is 8, to obtain the extract phase and the raffinate phase;
[0061] The extraction phase is rectified, the number of rectification towers is 20, the reflux ratio is 0.4, the operating pressure is 0.07 MPa, the operating temperature at the top of the rectifying tower is controlled within 90...
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