Slow stretching experimental device with high-temperature high-pressure circulating water and using method

A high temperature and high pressure, experimental device technology, applied in the field of material experimental research, can solve problems such as complex structure, troublesome maintenance, stress corrosion, etc., and achieve the effects of simple operation, low cost and stable operation

Active Publication Date: 2014-01-08
INST OF METAL RESEARCH - CHINESE ACAD OF SCI
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Problems solved by technology

[0003] The purpose of the present invention is to provide a slow tensile test device with high temperature and high pressure circulating water and its use method, which can test the stress cor

Method used

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  • Slow stretching experimental device with high-temperature high-pressure circulating water and using method
  • Slow stretching experimental device with high-temperature high-pressure circulating water and using method
  • Slow stretching experimental device with high-temperature high-pressure circulating water and using method

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[0072] Example 1

[0073] Slow tensile test of domestic nuclear grade 304 stainless steel in high temperature and high pressure circulating B+Li water at 300℃, 10MPa, and dissolved oxygen (DO) saturation.

[0074] The experimental material is sensitized domestic nuclear grade 304 stainless steel. The heat treatment system is 304 stainless steel in a solid solution state at 650℃ for 24 hours, followed by furnace cooling. According to ASTM E399, the processing thickness (B) of the 1 / 2T compact tensile specimen (CT specimen) is 12.5mm, the width (W) is 25mm, and the length (H) is 24mm. The surface of the 1 / 2T compact tensile specimen (CT specimen) is polished, and then fatigued in the air to produce a prefabricated 4mm long crack. Fix the sample on the fixture, tighten the autoclave, and pass the circulating solution. When the solution flows back to the water storage tank, then adjust the back pressure valve to make the pressure 10MPa, the preheater set temperature is 320°C, the au...

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Abstract

The invention belongs to the field of experimental researches on materials, and particularly discloses a slow stretching experimental device with high-temperature high-pressure circulating water and a using method. The device mainly comprises four parts, namely a high-temperature high-pressure circulating water system, a slow stretching loading device, a hydrochemical control system and a loading monitoring system, wherein the high-temperature high-pressure circulating water system can be used for providing a dynamic high-temperature high-pressure water environment; the slow stretching loading device is used for stretching a test sample in a high-pressure kettle at different strain rates; the hydrochemical control system is used for controlling hydrochemical parameters of the high-temperature high-pressure circulating water system; the loading monitoring system is used for regulating and recording a stretch curve of the test sample in the kettle; the test sample in the high-pressure kettle is fixedly arranged on a fixture; the fixture is connected to the upper end of a loading shaft, and an adapter coupling device is connected to the lower end of the loading shaft; a stretching tester is connected to the lower end of the adapter coupling device, and is used for realizing the slow strain rate loading of the test sample. According to the device and the method, the stress corrosion of a material can be tested in a high-temperature high-pressure circulating water environment, and the problems of complex structure, troublesome maintenance and the like in the prior art are solved.

Description

technical field [0001] The invention belongs to the field of material experiment research, more precisely, relates to a slow strain corrosion cracking experiment device with high temperature and high pressure circulating water and a use method. Background technique [0002] Nuclear power is an efficient and clean energy, and the development of nuclear power is an important way to solve the contradiction between my country's economic development and the unbalanced energy distribution. At present, commercial nuclear power plants mainly use light water reactors. Since the service environment of light water reactor nuclear power plants is high-temperature and high-pressure water (280-343°C, 8-16MPa), its pressure boundaries such as pressure vessels, steam generators, and main pipelines are subject to certain pressures. service stress. Practice has shown that stress corrosion cracking in high-temperature and high-pressure water in nuclear power service is one of the key issues a...

Claims

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Application Information

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IPC IPC(8): G01N3/56G01N17/00
Inventor 刘侠和吴欣强韩恩厚王翔
Owner INST OF METAL RESEARCH - CHINESE ACAD OF SCI
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