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A kind of preparation method and application of Muxiang Liqi tablet

A technology of making woody qi-relieving tablets and vinegar, which is applied to medical preparations containing active ingredients, pharmaceutical formulas, plant raw materials, etc., can solve the problems of large dosage for patients, rough process, and impact on application, and achieve the effect of reducing dosage

Inactive Publication Date: 2016-03-09
张红
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] In the prior art, there is no report about the use of supercritical and microwave technology in the extraction and preparation of Muxiang Liqi Tablets. However, the traditional Chinese medicine is directly powdered, extracted with volatile oil, and decocted in water. The process is rough and backward, and there are many impurities, resulting in excessive dosage for patients. Large, inconvenient to take, seriously affecting the clinical application of this product

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] Take 48g of woody incense, 96g of vinegar-made Cyperus cyperi, 96g of black medicine, 48g of vinegar-made green peel, 96g of tangerine peel, 96g of citrus aurantium, 96g of citrus aurantium, 96g of magnolia officinalis made from ginger juice, 24g of vinegar-made three-lens, 24g of vinegar-boiled curcuma, hawthorn 96g, betel nut 120g, evodia 12g, cinnamon 12g, nard pine 15g, bellflower 48g, scutellaria baicalensis 96g, rhubarb 48g, fried morning glory 48g. 2 In the supercritical extractor, ethanol is used as an entrainer, and the volume percentage of the entrainer to the total extraction solvent is 5%, the extraction pressure is 25MPa, the temperature is 40°C, and the CO 2 The flow rate is 2ml / g crude drug·min, the extraction time is 200min, and the supercritical extract is obtained for use; the rest of the traditional Chinese medicine is taken, pulverized, added 1.6L of 50% ethanol, and put into a microwave extraction device for microwave extraction. The extraction power...

Embodiment 2

[0034] Take 48g of woody incense, 96g of vinegar-made Cyperus cyperi, 96g of black medicine, 48g of vinegar-made green peel, 96g of tangerine peel, 96g of citrus aurantium, 96g of citrus aurantium, 96g of magnolia officinalis made from ginger juice, 24g of vinegar-made three-lens, 24g of vinegar-boiled curcuma, hawthorn 96g, betel nut 120g, evodia 12g, cinnamon 12g, nard pine 15g, bellflower 48g, scutellaria baicalensis 96g, rhubarb 48g, fried morning glory 48g. 2 In the supercritical extractor, ethanol is used as an entrainer, and the volume percentage of the entrainer in the total extraction solvent is 4%, the extraction pressure is 30MPa, the temperature is 50°C, and the CO 2 The flow rate is 3ml / g crude drug·min, the extraction time is 180min, and the supercritical extract is obtained for use; the rest of the traditional Chinese medicine is taken, pulverized, added 1.6L of 50% ethanol, and put into a microwave extraction device for microwave extraction. The extraction power...

Embodiment 3

[0037] Take 48g of woody incense, 96g of vinegar-made Cyperus cyperi, 96g of black medicine, 48g of vinegar-made green peel, 96g of tangerine peel, 96g of citrus aurantium, 96g of citrus aurantium, 96g of magnolia officinalis made from ginger juice, 24g of vinegar-made three-lens, 24g of vinegar-boiled curcuma, hawthorn 96g, betel nut 120g, evodia 12g, cinnamon 12g, nard pine 15g, bellflower 48g, scutellaria baicalensis 96g, rhubarb 48g, fried morning glory 48g. 2 In the supercritical extractor, ethanol is used as an entrainer, and the volume percentage of the entrainer to the total extraction solvent is 6%, the extraction pressure is 15MPa, the temperature is 30°C, and the CO 2The flow rate is 1ml / g crude drug·min, the extraction time is 220min, and the supercritical extract is obtained for use; the rest of the traditional Chinese medicine is taken, pulverized, added 1.6L of 50% ethanol, and put into a microwave extraction device for microwave extraction. The extraction power ...

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Abstract

The invention belongs to the technical field of traditional Chinese medicines, and particularly relates to a preparation method and application of a banksia rose qi-rectifying tablet. The banksia rose qi-rectifying tablet is prepared by supercritical extraction and microwave extraction of raw material medicines comprising 280 g of astragalus, 80 g of michelia hedyosperma lew, 190 g of angelica, 220 g of eclipta, 190 g of rhizoma atractylodis, 150 g of safflower, 140 g of radix paeoniae rubra, 140 g of peach kernel, 150 g of radix achyranthis bidentatae, 120 g of rhizoma ligustici wallichii, 70 g of bitter orange and 100 g of platycodon, and the content of baicalin is greatly improved. The present invention also provides the application of the banksia rose qi-rectifying tablet in preparation of drugs for inhibiting cell proliferation of mice breast cancer cell C127.

Description

technical field [0001] The invention belongs to the technical field of traditional Chinese medicine, and in particular relates to a preparation method and application of Muxiang Liqi Tablet. Background technique [0002] The standard number of Muxiang Liqi Tablets is WS-11113 (ZD-1113)-2002, which is recorded in the Spleen and Stomach Subvolume of the National Compilation of Chinese Patent Medicine Standards. 48g of woody incense, 96g of vinegar-made Cyperus cyperi, 96g of black medicine, 48g of vinegar-made green peel, 96g of tangerine peel, 96g of aurantium, 96g of citrus aurantium, 96g of magnolia from ginger juice, 24g of vinegar-made three-lens, 24g of vinegar-boiled curcuma, hawthorn 96g, betel nut 120g, evodia 12g, cinnamon 12g, nard pine 15g, bellflower 48g, scutellaria baicalensis 96g, rhubarb 48g, and fried morning glory 48g are made as raw materials. For qi stagnation and discomfort, loss of food and water, fullness in the chest and hypochondrium, abdominal fulln...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K36/9066A61K9/20A61P35/00A61P15/14A61P1/00A61P1/14A61P1/10
Inventor 张红张在芬岳妍秋孙雪
Owner 张红
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