Supercapacitor sizing manufacturing method
A supercapacitor and slurry technology, which is applied in the manufacture of hybrid/electric double layer capacitors, etc., can solve problems such as imperfect preparation methods, and achieve the effects of good slurry coating performance, increased energy density, and short dispersion time
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Embodiment 1
[0041] A method for preparing supercapacitor slurry, the method steps are as follows:
[0042] 1. Weigh LA133 and 20g CMC with a solid content of 50g, add them to 2800g deionized water, and stir for 30min with a vacuum stirrer;
[0043] 2. Add 200g of conductive carbon black while stirring, stir evenly and stir with a vacuum mixer for 30min;
[0044] 3. Then use a high-shear dispersing emulsifier to stir for 10 minutes at a speed of 20000r / min;
[0045] 4. Weigh 730g of activated carbon, add in order while stirring, stir with a vacuum mixer for 30min after stirring evenly;
[0046] 5. Then use a high-shear dispersing emulsifier to stir for 10 minutes at a speed of 20000r / min;
[0047] 6. Vacuumize and stir with a vacuum stirrer for 40 minutes to obtain the supercapacitor slurry.
[0048] figure 1 and figure 2 It is a scanning electron microscope (SEM) picture of the slurry. It can be seen from the figure that carbon black is evenly distributed between and on the activate...
Embodiment 2
[0050] A method for preparing supercapacitor slurry, the method steps are as follows:
[0051] 1. Weigh LA132 and 30g CMC with a solid content of 70g, add them to 2600g deionized water, and stir with a vacuum mixer for 30min;
[0052] 2. Add 300g of conductive carbon black while stirring, stir evenly and stir with a vacuum mixer for 30min;
[0053] 3. Then use a high-shear dispersing emulsifier to stir for 10 minutes at a speed of 20000r / min;
[0054] 4. Weigh 600g of ordered mesoporous carbon, add in order while stirring, and stir with a vacuum mixer for 30min after stirring evenly;
[0055] 5. Then use a high-shear dispersing emulsifier to stir for 10 minutes at a speed of 20000r / min;
[0056] 6. Vacuumize and stir with a vacuum stirrer for 40 minutes to obtain the supercapacitor slurry.
[0057] After SEM testing, it can be observed that the conductive carbon black is evenly distributed on the surface of the ordered mesoporous carbon.
Embodiment 3
[0059] A method for preparing supercapacitor slurry, the method steps are as follows:
[0060] 1. Weigh LA133 with a solid content of 4g and 1g of CMC, add it to 280g of deionized water, and stir for 10 minutes with a vacuum stirrer;
[0061] 2. Add 10g of conductive carbon black while stirring, stir evenly and then stir with a vacuum mixer for 10min;
[0062] 3. Then use a high-shear dispersing emulsifier to stir for 2 minutes at a speed of 20000r / min;
[0063] 4. Add 85g of graphene while stirring, stir evenly and stir with a vacuum mixer for 10min;
[0064] 5. Then use a high-shear dispersing emulsifier to stir for 5 minutes at a speed of 20000r / min;
[0065] 6. Vacuumize and stir with a vacuum stirrer for 20 minutes to obtain the supercapacitor slurry.
[0066] After SEM testing, it can be observed that the conductive carbon black is evenly distributed on the graphene surface.
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