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Steam dryness test method and device

A dryness and steam technology, which is applied in the analysis by chemical reaction of materials, and material analysis by observing the influence on chemical indicators, can solve the problem of high labor cost, unstable titration process speed, and determination of dryness. Error and other problems, to achieve the effect of simple operation, reducing the influence of human factors and the environment, and improving the accuracy

Active Publication Date: 2014-04-23
PETROCHINA CO LTD
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  • Abstract
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  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Because most of the commonly used testing methods use manual intervention, if there is a change in the color of condensed water, uneven mixing, unstable titration process speed, and changes in visual senses, etc., it will affect the measurement results and bring new problems to the determination of dryness. Large error and high labor cost; in addition, the assay method will have a certain hysteresis, when the steam dryness changes rapidly, it may not be able to respond in time

Method used

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  • Steam dryness test method and device

Examples

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Embodiment 1

[0048] Perform the following steps to measure steam dryness.

[0049] 1. Fold the qualitative filter paper into a trumpet shape, place it in a ¢75mm long-necked glass funnel, and insert the funnel into a 100ml Erlenmeyer flask A.

[0050] 2. Pour the steam condensed water sample into the funnel and let it pass through the qualitative filter paper into the Erlenmeyer flask A.

[0051] 3. Fix the micropump on the titration stand with a butterfly clip. And pour 0.05mol / l silver nitrate standard solution into the micropump.

[0052] 4. Place a 100ml beaker under the nozzle of the micropump, turn on the switch of the micropump, discharge the air from the lower part, and when the liquid level is aligned with a certain scale, turn off the switch immediately for use.

[0053] 5. Use a straight pipette and a suction ball to take an appropriate amount of filtered steam condensed water sample (10ml), and place it in an empty Erlenmeyer flask B.

[0054] 6. Add 2-3 drops of 1% phenolph...

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Abstract

The invention provides a method for testing steam dryness. The method comprises the following steps: placing a steam condensate sample in a reactor; under the condition of continuously stirring and mixing reaction liquor by an automatic stirrer, continuously titrating silver nitrate liquor into the reactor by a micro-pump and monitoring the use level of the silver nitrate liquor; continuously monitoring the light transmittance in the titrating process by a transmissometer and automatically generating a light transmittance-silver nitrate titer curve, wherein the monitoring is at least carried out till the light transmittance is stable; and determining a reaction equivalent point from the curve so as to obtain the use level of the silver nitrate liquor at the equivalent point, and calculating the content of chlorine ions in the steam condensate sample so as to obtain the steam dryness by means of the content of chlorine ions. The invention further relates to a steam dryness test device which implements the method.

Description

technical field [0001] The invention relates to the field of petroleum exploitation, in particular to an assay method and device for measuring steam dryness during steam injection in an oil field. Background technique [0002] In the current heavy oil production, the steam injection huff and puff thermal recovery method is often used. The main process is to inject high-dryness steam into the oil layer, thereby realizing the heating of the heavy oil, and using high temperature to reduce the viscosity of the heavy oil, thereby performing huff and puff oil recovery. It is very important to monitor the dryness of steam in the thermal recovery process of heavy oil. The detection results can be used to determine the required steam injection amount and steam injection time, so as to improve oil recovery efficiency. [0003] General steam is composed of completely gaseous steam and liquid water droplets, and steam quality refers to the percentage of "dry steam" (that is, completely...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/79
Inventor 邓中先步新兵朱强金璐黄丽乔沐王喆刘国忠
Owner PETROCHINA CO LTD
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