Environment-friendly flame-retardant silicate adhesive for bamboo woods and preparation method thereof
A silicate and adhesive technology, applied in the direction of adhesives, adhesive additives, inorganic adhesives, etc., can solve the problems of glued state damage, veneer rupture, loss rate increase, etc., to ensure environmental protection and water resistance Excellent, dimensionally stable effect
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Embodiment 1
[0034] A preparation method of an environmentally friendly flame-retardant silicate adhesive for bamboo and wood, comprising the following steps:
[0035] 1) Add 60 parts by weight of water glass into a 200ml beaker, stir it with an electric stirring device for about 5 minutes at room temperature, then add 5 parts by weight of HPP-101 hyperbranched polyphosphate resin into the water glass, at a speed higher than 20 rpm The rotating speed of / second stirs 20-25min, makes resin and water glass mix rapidly, obtains pale yellow hyperbranched polyphosphate-water glass mixture;
[0036] 2) Add 6 parts by weight of cooked glutinous rice flour to the mixture obtained in step 1), stir at a speed lower than 8 rpm for 10 minutes, and then stir at a speed higher than 20 rpm for 15 minutes to obtain glutinous rice flour thickened Hyperbranched polyphosphate-water glass mixture;
[0037] 3) Add 5 parts by weight of nano-attapulgite to 10 parts by weight of nano-SiO with a mass fraction of...
Embodiment 2
[0040] A preparation method of an environmentally friendly flame-retardant silicate adhesive for bamboo and wood, comprising the following steps:
[0041] 1) Add 65 parts by weight of water glass into a 200ml beaker, stir with an electric stirring device for about 5 minutes at room temperature, and then add 6.5 parts by weight of HPP-102 hyperbranched polyphosphate resin into the water glass, at a speed higher than 20 rpm The rotating speed of / second stirs 20-25min, makes resin and water glass mix rapidly, obtains pale yellow hyperbranched polyphosphate-water glass mixture;
[0042] 2) Add 4.5 parts by weight of cooked glutinous rice flour to the mixture obtained in step 1), stir at a speed lower than 8 rpm for 10 minutes, and then stir at a speed higher than 20 rpm for 15 minutes to obtain glutinous rice flour thickened Hyperbranched polyphosphate-water glass mixture;
[0043] 3) Add 7.5 parts by weight of nano-attapulgite to 15 parts by weight of nano-SiO with a mass frac...
Embodiment 3
[0046] A preparation method of an environmentally friendly flame-retardant silicate adhesive for bamboo and wood, comprising the following steps:
[0047]1) Add 70 parts by weight of water glass into a 200ml beaker, stir with an electric stirring device for about 5 minutes at room temperature, and then add 8 parts by weight of HPP-103 hyperbranched polyphosphate resin into the water glass, at a speed higher than 20 rpm The rotating speed of / second stirs 20-25min, makes resin and water glass mix rapidly, obtains pale yellow hyperbranched polyphosphate-water glass mixture;
[0048] 2) Add 3 parts by weight of cooked glutinous rice flour to the mixture obtained in step 1), stir at a speed lower than 8 rpm for 10 minutes, and then stir at a speed higher than 20 rpm for 15 minutes to obtain glutinous rice flour thickened Hyperbranched polyphosphate-water glass mixture;
[0049] 3) Add 10 parts by weight of nano-attapulgite to 20 parts by weight of nano-SiO with a mass fraction o...
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