Insulated and flame-retardant nylon composite material with high thermal conductivity and preparation method thereof
A flame-retardant nylon and composite material technology, applied in the field of intelligent polymer materials, can solve the problems of poor flame-retardant effect, limited application, non-insulation, etc., and achieve the effects of simple and easy preparation process, excellent mechanical properties, and good insulation
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[0045] A preparation method of high thermal conductivity insulating flame retardant nylon composite material, comprising the following steps:
[0046] 1) Soak magnesium nitride in an ethanol solution with a mass percentage of 1-3% silane coupling agent KH560 for 3-8 minutes, and volatilize to remove ethanol;
[0047] 2) Melt extrusion and granulation of nylon 6 and magnesium nitride treated in step 1) through a twin-screw extruder to obtain thermally conductive master batches;
[0048] 3) Melt extrusion and granulation of nylon 66 and glass fiber through a twin-screw extruder to obtain a reinforced masterbatch;
[0049] 4) Mix ultra-fine light magnesium carbonate, light magnesium oxide, magnesium hydroxide and 1-3% KH560 ethanol solution in a high-speed mixer for 3-8 minutes at a temperature of 50-70°C;
[0050] 5) Add the thermally conductive masterbatch and the reinforced masterbatch into the high-speed mixer in step 4), and mix for 25-30 minutes at a temperature of 50-70°C...
Example Embodiment
[0055] Example 1
[0056] 1) Soak the magnesium nitride in an ethanol solution with a mass percentage of 2% KH560 for 5 minutes, and volatilize to remove the ethanol;
[0057] 2) Melt extrusion and granulation of nylon 6 and magnesium nitride treated in step 1) through a twin-screw extruder to obtain thermally conductive master batches;
[0058] 3) Melt extrusion and granulation of nylon 66 and glass fiber through a twin-screw extruder to obtain a reinforced masterbatch;
[0059] 4) Mix ultrafine light magnesium carbonate, light magnesium oxide, magnesium hydroxide and 2% KH560 ethanol solution in a high-speed mixer for 5 minutes at a temperature of 60°C;
[0060] 5) Add the thermally conductive masterbatch and the reinforced masterbatch to the high-speed mixer in step 4), mix for 25 minutes, and the temperature is 60°C;
[0061] 6) Place the raw material, elastomer and antioxidant mixed in step 5) in a twin-screw extruder, melt extrusion and granulation to obtain a high th...
Example Embodiment
[0065] Example 2
[0066] 1) Soak the magnesium nitride in an ethanol solution with a mass percentage of 2% KH560 for 5 minutes, and volatilize to remove the ethanol;
[0067] 2) Melt extrusion and granulation of nylon 6 and magnesium nitride treated in step 1) through a twin-screw extruder to obtain thermally conductive master batches;
[0068] 3) Melt extrusion and granulation of nylon 66 and glass fiber through a twin-screw extruder to obtain a reinforced masterbatch;
[0069] 4) Mix ultrafine light magnesium carbonate, light magnesium oxide, magnesium hydroxide and 2% KH560 ethanol solution in a high-speed mixer for 8 minutes at a temperature of 60°C;
[0070] 5) Add the thermally conductive masterbatch and the reinforced masterbatch to the high-speed mixer in step 4), mix for 25 minutes, and the temperature is 60°C;
[0071] 6) Place the raw material, elastomer and antioxidant mixed in step 5) in a twin-screw extruder, melt extrusion and granulation to obtain a high t...
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