Method for preparing novel polycarboxylic acid retarded high-performance water reducer
A polycarboxylic acid, high-performance technology, used in the preparation of new CM-8 polycarboxylic acid retarding high-performance water reducing agent, can solve the problems of insufficient dispersibility, poor fluidity, low strength, etc. Many variables, strong slump retention ability, good dispersion effect
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[0007] A preparation method of a novel CM-8 polycarboxylic acid retarding high-performance water reducer, comprising a first reaction kettle, a second reaction kettle, and 0.31% to 0.51% of ammonium persulfate and 0.11% to 0.32% of mercaptoethanol A material made of 54% to 60% deionized water is characterized in that 12.5% to 14.5% of methoxypolyethylene glycol and 2.7% to 3.5% of methacrylic acid, add 0.055% to 0.093% phenothiazine to the first reaction kettle after adding the temperature to 75°C, add 0.059% to 0.091% phenothiazine, and then heat up to 85°C to the first reaction kettle Add 0.188% to 0.235% sulfuric acid (98%) to the kettle. After adding 0.188% to 0.235% sulfuric acid (98%), continue to heat up to 125°C and start constant temperature for 5 hours. The constant temperature is controlled at 125±6°C After the constant temperature is completed, the intermediate product of the ester macromonomer containing unsaturated double bonds is obtained, the macromonomer int...
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