A kind of preparation method of yttrium silicate ceramic powder

A ceramic powder, yttrium silicate technology, applied in coating, metal material coating process, melt spraying and other directions, can solve the problem of difficult to obtain a single crystal product and other problems, achieve stable pH value, high purity, guaranteed The effect of purity
CN104003699BActive Publication Date: 2016-08-17CENT SOUTH UNIV
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Patent Information

Authority / Receiving Office
CN ยท China
Patent Type
Patents(China)
Current Assignee / Owner
CENT SOUTH UNIV
Publication Date
2016-08-17

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Abstract

The invention relates to a preparation method of yttrium silicate ceramic powder, in particular relates to a preparation method of yttrium silicate ceramic powder for environment barrier coating, and belongs to the technical field of oxide ceramic material preparation. The method comprises the following steps: using a yttrium solution with Y<3+> ion concentration of 0.6-1.5 mol / L as solution A; weighing silicate ester according to a molar ratio of Y to Si being 2: 1; adding alcohol and water in the weighed silicate ester according to a volume ratio of the silicate ester to alcohol to water being 1: 1-2: 2-6 to obtain solution B; uniformly mixing the solutions A and B solution to obtain the mixed solution containing aluminum and silicon; adding the mixed solution containing aluminum and silicon into ammonium hydroxide with pH value of 9-10 at a speed of dropwise adding 0.2-0.5 L of the mixed solution containing aluminum and silicon in 1L of precipitator every minute, and stirring to obtain the co-precipitate; after the reaction is finished, standing, filtering, washing and drying the residue, calcining for at least 4 hours at 800-1000 DEG.C to obtain the Y2SiO5 ceramic composite powder. The method provided by the invention is short in reaction period and good in repeatability; and the obtained product is high in purity and is of a single crystal form.
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Description

technical field

[0001] The invention relates to a preparation method of yttrium silicate ceramic powder, in particular to a preparation method of yttrium silicate ceramic powder for an environmental barrier coating, belonging to the technical field of oxide ceramic material preparation. The composite powder is used to prepare an environmental barrier coating, and is suitable for high temperature protection on the surface of silicon-based materials such as C / C-SiC composite materials and silicon nitride. technical background

[0002] Carbon / carbon-silicon carbide (C / C-SiC) composite material is a ceramic matrix composite material with carbon fiber as the reinforcing phase, which combines the superior mechanical properties of fiber reinforcement and the good chemical and thermal stability of ceramics, and has a high specific Strong, high specific modulus, low density, good oxidation resistance, corrosion resistance, excellent mechanical properties and thermophysical properties...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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