The invention discloses a method for rapidly measuring
arsenic element in grain by an X fluorescent spectrometry. The method comprises the steps of step one, manufacturing a
standard curve of a standard sample, namely sieving a series of
arsenic grain
powder with standard content gradient, putting the sieved
powder into a sample cup and compacting; scanning a series of standard sample on a
machine to obtain the X
fluorescence intensity of the standard sample with known content, and calibrating the
standard curve; and step two, treating a sample to be measured, namely removing peels of a certain amount of taken grain,
grinding and sieving; packaging the taken
powder into the sample cup and compacting to form the sample to be measured, wherein the amount of the powder is equal to that of the powder in the step one; testing by a
machine, and calculating the content. Due to adoption of the method, the current detection accuracy and the
repeatability are optimized, so that the high accuracy of the test results, good regularity and good evenness are guaranteed; meanwhile, the treatment method is simple, and only a hammer type
cyclone grinder is used for
grinding and sieving the sample, so that the time is short, and the pretreatment of the sample only needs 2 seconds; the instrument can test simply and can be operated by a key, no instrument exists,
environmental protection is realized, and waste consumable is not produced.