Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Preparation method of rosin glyceride

A technology of rosin glycerides and glycerin, which is applied in the field of preparation of rosin glycerides, can solve the problems of memory loss, damage, and the failure of rosin glycerides to meet the requirements of food additive standards, and achieve the reduction of the content of trace metal elements such as aluminum, simple operation, The effect of mild reaction conditions

Inactive Publication Date: 2014-09-10
陈昆
View PDF3 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, because rosin has not removed trace metal elements in the preparation process, the raw material rosin bought from the market generally contains high trace metal elements such as aluminum, and these trace metal elements are too high to cause brain damage and memory loss , senile dementia and other consequences, this is a relatively sensitive impurity that affects the application of rosin in food additives with extremely strict requirements
If these rosins containing trace metal elements such as aluminum on the high side are used as one of the raw materials to prepare rosin glycerides, the obtained product contains trace metal elements such as aluminum must also be high, which will make its product rosin glycerides Unable to meet the requirements of food additive standards

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] A preparation method of rosin glyceride, the method comprising the following preparation steps:

[0015] A. Put 10Kg of raw material rosin into 20Kg of acidic solution with a pH value of 3, then add 0.15Kg of sodium citrate to it, stir evenly, then heat to 80°C for heat preservation reaction for 20min, after the reaction, stand still and separate , to obtain refined rosin;

[0016] B, the rosin that 2.5Kg fumaric acid, 0.5Kg water and step A make are put into reactor and mix evenly, then be heated to 180 ℃ and carry out insulation reaction for 3 hours;

[0017] C. After the reaction described in step B is completed, add 3.3Kg of glycerin to the reaction kettle, mix well, and then heat to 265° C. for heat preservation reaction for 4 hours to obtain rosin glyceride.

[0018] The aluminum content in the rosin glyceride prepared in this embodiment is 7.5ppm.

Embodiment 2

[0020] A preparation method of rosin glyceride, the method comprising the following preparation steps:

[0021] A. Put 30Kg of raw material rosin into 60Kg of acidic solution with a pH value of 3.5, then add 0.72Kg of sodium citrate to it, stir evenly, then heat to 90°C for 17 minutes of heat preservation reaction, after the reaction, stand still and separate , to obtain refined rosin;

[0022] B, the rosin that 9.4Kg fumaric acid, 3.4Kg water and step A make are put into reactor and mix evenly, then be heated to 180 ℃ and carry out insulation reaction 3 hours;

[0023] C. After the reaction described in step B is completed, add 10Kg of glycerin to the reaction kettle, mix well, then heat to 265° C. for heat preservation reaction for 4 hours to obtain rosin glyceride.

[0024] The aluminum content in the rosin glyceride prepared in this embodiment is 7.4ppm.

Embodiment 3

[0026] A preparation method of rosin glyceride, the method comprising the following preparation steps:

[0027] A. Put 10Kg of raw material rosin into 20Kg of acidic solution with pH value of 4, then add 0.3Kg of sodium citrate to it, stir evenly, then heat to 95°C for insulation reaction for 15min, after the reaction, stand and separate , to obtain refined rosin;

[0028] B, the rosin that 3Kg fumaric acid, 1.25Kg water and step A make are put into reactor and mix evenly, then be heated to 180 ℃ and carry out insulation reaction for 3 hours;

[0029] C. After the reaction described in step B is completed, add 3.3Kg of glycerin to the reaction kettle, mix well, and then heat to 265° C. for heat preservation reaction for 4 hours to obtain rosin glyceride.

[0030] The aluminum content in the rosin glyceride prepared in this embodiment is 7.2ppm.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses a preparation method of rosin glyceride, and belongs to the technical field of deep processing of rosin. According to the invention, pine resin is used as a raw material and is prepared into rosin by virtue of the following steps: firstly, removing trace metal elements such as aluminum; then, enabling the trace metal element removed pine resin to be subjected to modified reaction with fumaric acid and water; finally, enabling the reaction product to be subjected to esterification reaction with glycerin to obtain a product, namely rosin glyceride. The method is simple in operation, mild in reaction condition, capable of effectively reducing the content of the trace metal elements such as aluminum and the like in rosin glyceride as the product, incapable of injuring human bodies and capable of being up to the standard of a food additive.

Description

technical field [0001] The invention belongs to the technical field of rosin deep processing, and in particular relates to a preparation method of rosin glyceride. Background technique [0002] As a food additive, rosin glyceride can be used as a base agent for gummies because of its excellent emulsifying properties, and can endow gummies with foaming, plasticizing, and chewing properties; it is used in bubble gum, chewing gum, chewing gum, Sugar-free chewing gum, with good taste, anti-oxidation, and softness; it can also be used as an emulsion stabilizer in beverages. [0003] However, because rosin has not removed trace metal elements in the preparation process, the raw material rosin bought from the market generally contains high trace metal elements such as aluminum, and these trace metal elements are too high to cause brain damage and memory loss , senile dementia and other consequences, this is a relatively sensitive impurity that affects the application of rosin in f...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C09F1/04
Inventor 陈昆
Owner 陈昆
Features
  • Generate Ideas
  • Intellectual Property
  • Life Sciences
  • Materials
  • Tech Scout
Why Patsnap Eureka
  • Unparalleled Data Quality
  • Higher Quality Content
  • 60% Fewer Hallucinations
Social media
Patsnap Eureka Blog
Learn More

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2025 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com