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A kind of extraction method of the active ingredient of sour lychee ethanol part

A technology of active ingredients and extraction methods, which is applied in the field of extraction of active ingredients from the ethanol part of sour lychee, can solve the problems of unclear pharmacological effects, unspecific, slow curative effect, etc., and achieve the effects of stable extraction results, easy consumption, and high extraction rate

Active Publication Date: 2016-08-17
右江民族医学院
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

One of the characteristics of traditional Chinese medicine is compound medicine, which is characterized by multi-target, multi-site, and multi-level comprehensive effects. The curative effect is slow and not specific, and the pharmacological effects are not clear. Correspondingly extract active ingredients according to specific conditions.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] The sour litchi core, leaves, stems, bark and pericarp are dried respectively, pulverized, and passed through a 40-mesh sieve; 10g is weighed and added to different extractors, and then 200ml of 95% ethanol is added, stirred evenly with a glass rod, Soak time is 0.3 hour, carry out microwave extraction, microwave power is 500W, and time is 90 seconds; Filter extract respectively, underpressure distillation, control temperature is 70 ℃, and vacuum degree is-0.1MPa, obtain extract, reclaim Ethanol; respectively open the bottle cap of the extract, control the temperature in a water bath at 70°C, and volatilize the extract until there is no alcohol smell; dissolve the extract in n-butanol saturated with water respectively, filter to get the upper layer, distill under reduced pressure, and control the temperature to 70°C and a vacuum of -0.1MPa to make a clear ointment and recover n-butanol; respectively open the bottle cap of the clear ointment, control the temperature in a ...

Embodiment 2

[0035] The sour litchi core, leaves, stems, bark and pericarp are dried respectively, pulverized, and passed through a 40-mesh sieve; 10g is weighed and added to different extractors, and then 200ml of 95% ethanol is added, stirred evenly with a glass rod, Soak time is 0.2 hour, carry out microwave extraction, microwave power is 500W, time is 80 seconds; Filter extract, decompression distillation, control temperature is 70 ℃, and vacuum degree is-0.1MPa, obtain extract, reclaim ethanol ; Open the bottle cap of the extract, control the temperature in a water bath at 70°C, and volatilize the extract until there is no alcohol smell; dissolve the extract in n-butanol saturated with water, filter the upper layer, distill under reduced pressure, and control the temperature at 70°C , the vacuum degree is -0.1MPa, make clear ointment, reclaim n-butanol; open the bottle cap of clear ointment respectively, control temperature 70 ℃ in water bath, volatilize clear ointment until there is n...

Embodiment 3

[0040]The sour litchi core, leaves, stems, bark and pericarp are dried respectively, pulverized, and passed through a 40-mesh sieve; 10g is weighed and added to different extractors, and then 200ml of 95% ethanol is added, stirred evenly with a glass rod, The soaking time is 0.4 hour, and microwave extraction is carried out, the microwave power is 400W, and the time is 100 seconds; filter the extract respectively, and distill under reduced pressure, the control temperature is 70 ° C, and the vacuum degree is -0.1MPa to obtain the extract and recover Ethanol; respectively open the bottle cap of the extract, control the temperature in a water bath at 70°C, and volatilize the extract until there is no alcohol smell; dissolve the extract in n-butanol saturated with water respectively, filter to get the upper layer, distill under reduced pressure, and control the temperature to 70°C and a vacuum of -0.1MPa to make clear ointment and recover n-butanol; open the bottle cap of the clea...

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Abstract

The invention discloses a method for extracting an effective component from an ethanol part of acid litchi. The method comprises the following steps: baking and crushing acid litchi, soaking in 95% ethanol for 0.2-0.4 hour, extracting for 80-100 seconds with microwave power of 400-600W, and concentrating to obtain an extract; recovering the ethanol, and dissolving the extract with n-butyl alcohol, filtering, concentrating at reduced pressure to prepare a clear extract, namely the total active component of acid litchi, and recovering the n-butyl alcohol, wherein the acid litchi is acid litchi kernels, acid litchi leaves, acid litchi stems, acid litchi barks and acid litchi fruit peels. The method has the characteristics of simple and effective extraction and purification and high extraction rate; the extract is definite in component and high in purity, and can be used for preparing preparations which have better curative effect and are convenient to take; a solvent for extraction is absolute ethyl alcohol, the step of configuring concentration is cancelled, the time is saved, and the recovered solvent can be used in other aspects. The method is economic, energy-saving and environment-friendly, is advantageous to production performance, and has good economical benefit, social benefit and ecological benefit.

Description

technical field [0001] The invention belongs to the technical field of extracting traditional Chinese medicines, and relates to a method for extracting active ingredients from ethanol parts of sour lychees. Background technique [0002] Sour litchi is a Sapindaceae plant sour litchi (Litchi Chinensis Sonn), mainly produced in Guangdong, Guangxi and other places. The effect of cold pain relief is recorded in multiple editions of "Chinese Pharmacopoeia". Active components such as polysaccharides, total saponins and flavonoids can be isolated from litchi and litchi cores. Studies have shown that litchi and litchi cores and their active components have the functions of blocking the synthesis of nitrosamines and scavenging nitrite ions, anti-oxidation and In addition to scavenging free radicals and inhibiting the biological activities of HBsAg, HBeAg and HBV-DNA, etc., it also has anti-inflammatory, analgesic, antipyretic and inhibition of transplanted tumors in mice, anti-immun...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K36/77
Inventor 钱力陈秉仆黄祖良莫小强韦贤陆海峰李容
Owner 右江民族医学院
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