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A kind of dyeing method of pure cotton black yarn resistant to mercerized strong alkali

A dyeing method and yarn technology, which is applied in the dyeing field of pure cotton black yarn, can solve the problems of high dye content and COD value, inability to withstand post-mercerizing strong alkali, and difficult wastewater treatment, etc., and achieve good dye promotion rate, The effect of less dye consumption and excellent dye compatibility

Active Publication Date: 2016-08-24
ANHUI HUAMAO TEXTILE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the structural characteristics of this kind of dyes, most of the active groups are bis-chloro-s-triazine structure, which determines its alkali resistance, but the promotion rate is poor and the dyeing rate is low.
At present, all dye manufacturers do not have this type of black dye. Dyeing companies use high-temperature yellow, navy blue, and red color matching when dyeing black. The amount of dye is large, and the weight of the dye to the fabric is more than 10% owf. The dyeing rate is low, the dye content and COD value in the waste liquid after dyeing are high, and the wastewater treatment is difficult; the dyeing temperature is as high as 80°C, and the energy consumption is large, so the dyeing cost is high
Although the general traditional medium-temperature reactive black dyes have good promotion rate, high dyeing rate, and low dyeing temperature of 60°C, most of them are composed of C.I. C.I. 82 orange with oxazine active group structure is blended, it is not alkali-resistant, so the fabric woven from pure cotton black yarn dyed with this type of reactive dye cannot withstand post-mercerizing strong alkali treatment

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • A kind of dyeing method of pure cotton black yarn resistant to mercerized strong alkali

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] Example 1: Black yarn with orange light

[0021] The pre-treatment of pure cotton yarn is carried out by the conventional one-step pretreatment process of de-boiling and bleaching. Put the pre-treated pure cotton yarn in the large liquid flow skein dyeing vat, close and tighten the dyeing vat door, fill it with soft water, add 0.5g / L sodium hexametaphosphate into the expansion vat when the temperature is raised to 40℃. Warm up to 50℃; use 3.0% owf reactive black G dye as the main dye, and 0.2% owf reactive red S-3B dye, 0.8% owf reactive yellow TS-3R dye, mix evenly to form a reactive dye solution, dyeing bath ratio 1:10; evenly add the prepared dye solution within 20 minutes, control the heating rate at 1°C / min to raise the temperature to 60°C, keep it warm for 15 minutes, and add 80g / L yuan manually and evenly in the self-expanding tank within 20 minutes Bright powder, heat preservation for 30 minutes, add 20g / L soda ash from the chemical material tank within 30 minutes...

Embodiment 2

[0022] Example 2: Black yarn with partial purple light

[0023] The pre-treatment of pure cotton yarn is carried out by the conventional one-step pretreatment process of de-boiling and bleaching. Put the pre-treated pure cotton yarn in the large liquid flow skein dyeing vat, close and tighten the dyeing vat door, fill it with soft water, add 0.5g / L sodium hexametaphosphate into the expansion vat when the temperature is raised to 40℃. Warm up to 50℃; use 6% owf reactive black G dye as the main dye, mix with 1% owf reactive red S-3B dye and 0.2% owf reactive navy blue SG dye to form a reactive dye solution with a dyeing bath ratio of 1 : 20; Evenly add the prepared dye solution within 20 minutes, control the heating rate at 1°C / min to raise the temperature to 60°C, keep it warm for 15 minutes, and manually add 80g / L sodium sulfate in the self-expanding tank within 20 minutes , Keep holding for 30 minutes, add 20g / L soda ash from the chemical material tank within 30 minutes, and dr...

Embodiment 3

[0024] Example 3: Greenish black yarn

[0025] The pre-treatment of pure cotton yarn is carried out by the conventional one-step pretreatment process of de-boiling and bleaching. Put the pre-treated pure cotton yarn in the large liquid flow skein dyeing vat, close and tighten the dyeing vat door, fill it with soft water, add 0.5g / L sodium hexametaphosphate into the expansion vat when the temperature is raised to 40℃. Heat up to 50℃; use 4.5% owf reactive black G dye as the main dye, and 0.3% owf reactive yellow TS-3R dye, 0.5% owf reactive navy blue SG dye, and mix them to form a reactive dye solution with a dyeing bath ratio of 1 : 15; Evenly add the prepared dye solution within 20 minutes, control the heating rate at 1°C / min to heat up to 60°C, keep it warm for 15 minutes, and manually add 80g / L sodium sulfate in the self-expanding tank within 20 minutes , Keep holding for 30 minutes, add 20g / L soda ash from the chemical material tank within 30 minutes, and drain the color aft...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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PUM

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Abstract

The invention discloses a dyeing method of pure cotton black yarn resistant to post-mercerized strong alkali, which comprises dyeing solution preparation, dyeing, soaping twice, hot water washing three times, pickling, softening, squeezing and drying processes. The medium-temperature reactive dye with multi-reactive group structure replaces the high-temperature reactive dye, which has good dye promotion rate, high color yield, excellent dye compatibility, low dyeing temperature, less dye consumption, and reduced dyeing cost. The pure cotton after dyeing is black The color fastness to alkali staining is greatly improved after the yarn is washed with the soap solution containing the diffusing agent N, and then treated with the reactive color fixing agent OS, the yarn has good resistance to mercerizing and strong alkali, and has relatively good performance in actual production. Strong application value. After being dyed by this dyeing method, the alkali fastness of the pure cotton black yarn is a color fastness of 4-5 grades, and a staining fastness of 4 grades, and the alkali fastness index of the colored yarn meets the requirements of the national standard.

Description

Technical field [0001] The invention relates to a dyeing method of mercerized color thread, in particular to a dyeing method of pure cotton black yarn resistant to post-mererization and strong alkali. Background technique [0002] The pure cotton high-count yarn is processed by singeing, mercerizing, dyeing and other processing steps to produce silk-like bright luster, soft and wrinkle-resistant high-quality mercerized dyed yarn. The knitted fabric woven with this yarn is processed twice After singeing, post mercerizing, softening and other processes, it becomes a high-grade pure cotton mercerized fabric. This "double-filament and double-burning" pure cotton mercerized fabric not only completely retains the excellent natural characteristics of raw cotton fiber, but also has silky luster, soft feel, good moisture absorption and breathability, full elasticity and drape; plus Rich in patterns and colors, comfortable and casual to wear, which fully reflects the temperament and taste...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06P1/38D06P1/673D06P3/66D06P5/02D06P5/04
Inventor 方长国杨蓓章军
Owner ANHUI HUAMAO TEXTILE
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